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PXPd-catalyzed borylation of aniline derivatives

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Wheaton S., Humanayun Kabir S., Zhang H., Vogels C., Decken A., Westcott S.
Open Chemistry
|
2010
|
vol. 8
|
issue 4
725-731
EN
Addition of pinacolborane (HBO2C2Me4) to 2-iodoaniline can be catalyzed using a number of palladium complexes, including [(t-Bu)2PCl]2PdCl2 (PXPd), to give the corresponding boronate ester 2-H2NC6H4(BO2C2Me4) in excellent yields. The PXPd system could also be used in the catalyzed borylation of substituted anilines to give the corresponding aminoboronate esters in moderate to high yields. [...]
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