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The Influence of Preparation Methods on Magnetic Properties of Fe/SiO₂ Soft Magnetic Composites

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Füzerová J., Füzer J., Kollár P., Kabátová M., Dudrová E.
Acta Physica Polonica A
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2017
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vol. 131
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issue 4
816-818
EN
An analysis of several variants of the Fe/polymer/SiO₂ composites in terms of the impact of iron powder particle shape (irregular, spherical), of the content (0.4-2.0 wt%), of the polymer type (shellac, thermoset SL450) and the method of its application as well as the effect of the preparation procedure of the composites (mixing and/or vacuum-pressure impregnation) on properties of electrical insulating layer (thickness and coherence), electrical resistivity and magnetic properties was carried out. It was found that the main governing factor of the microstructure formation is the shape, surface microgeometry of the iron particles and the insulator layer. These determine not only the uniformity of thickness and cohesion of the insulating layer of the applied polymer or its hybrid modification (polymer+SiO₂ nanoparticles), but also the most suitable method of preparation in terms of the achieved values of electrical and magnetic properties of the composites.
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Preparation and Characterization of Fe/SiO_{2} Powder Composites Using Impregnation Method

100%
Kabátová M., Füzer J., Füzerová J., Dudrová E., Kollár P.
Acta Physica Polonica A
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2014
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vol. 126
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issue 1
134-135
EN
Fe/SiO_{2} powder composite materials based on irregularly and/or spherically shaped iron powder particles with an addition of SiO_{2} nanopowder were prepared in two ways, (i) by mixing the Fe/SiO_{2} powder with 1.0 wt.% of Shellac dissolved in ethanol and (ii) by vacuum/pressure impregnation of low-temperature sintered Fe/SiO_{2} components with shellac dissolved in ethanol and with thermoplast SL450. SiO_{2} was implemented either as nanopowder or by sol-gel coating. Vacuum/pressure impregnation (VPI) of pre-sintered samples was performed in a steel container. The influence of iron particle shape and processing conditions on the electro-insulating layer was microscopically evaluated and correlated with the values of the electrical resistivity and coercivity. It has been found that the continuity, distribution and thickness of insulating phase is strongly controlled by the shape of iron particles. Using the VPI procedure, the irregular surface of iron particles may cause discontinuities of insulating layer, while the spherical iron particles are well covered with continuous evenly distributed insulating layer.
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