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  1. 1 Open Chemistry

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  1. 1 2008

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  1. 1 Baykal A.

  2. 1 Toprak M.

  3. 1 Özkaya T.

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2-pyrrolidone - capped Mn3O4 nanocrystals

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Özkaya T., Baykal A., Toprak M.
Open Chemistry
|
2008
|
vol. 6
|
issue 3
465-469
EN
Water-soluble Mn3O4 nanocrystals have been prepared through thermal decomposition in a high temperature boiling solvent, 2-pyrrolidone. The final product was characterized with XRD, SEM, TEM, FTIR and Zeta Potential measurements. Average crystallite size was calculated as ∼15 nm using XRD peak broadening. TEM analysis revealed spherical nanoparticles with an average diameter of 14±0.4 nm. FTIR analysis indicated that 2-pyrrolidone coordinates with the Mn3O4 nanocrystals only via O from the carbonyl group, thus confining their growth and protecting their surfaces from interaction with neighboring particles. [...]
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