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Hydride generation atomic absorption spectrometry with insitu graphite tube trapping for the determination of Se (IV) and Se (VI) in baltic sea water samples

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Niedzielski P., Siepak M., Dudzińska-Huczuk B.

Open Chemistry

2003

vol. 1

issue 3

314-324

This paper reports the results of an optimisation study for a procedure to determine the total selenium and its inorganic species, Se(IV) and Se(VI) using atomic absorption spectrometry combined with hydride generation and in-situ trapping of the analyte on the inner walls of the graphite tube. With the use of the proposed modification, a detection limit (3σ) of 0.018 ng/ml is achieved. This paper presents exemplary results, according to the proposed procedure, for selenium determination in samples of marine water. The concentrations of selenium in the samples ranged from <0.02 ng/ml to 0.16ng/ml of Se(IV) and from <0.02 ng/ml to 0.10 ng/ml of Se(VI).

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1 Open Chemistry

1 2003

1 Dudzińska-Huczuk B.

1 Niedzielski P.

1 Siepak M.

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Hydride generation atomic absorption spectrometry with insitu graphite tube trapping for the determination of Se (IV) and Se (VI) in baltic sea water samples