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Imaging of Magnetic Domains and Domain Walls in Spherical Fe-Si Powder Using Magnetic Force Microscopy

100%
Strečková M., Baťková M., Baťko I., Hadraba H., Bureš R.
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vol. 126
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issue 1
92-93
EN
The commercial Fe-Si powder, produced by Högänes Corporation, represents promising soft magnetic material for technological applications. The powder consists of spherical particles with diameter up to 150 μm. Internal microstructure of the powder is formed by grains of diameter of about 30 μm. Each separate grain has a random orientation of the easy magnetization axis and is sufficiently large to split into several magnetic domains. A comparative study of the atomic force microscopy (AFM) topography and the corresponding magnetic force microscopy (MFM) images was employed in order to examine the correlation between the grain size, boundaries of grains and characterization of the magnetic domains, which gives us an important knowledge about possible behavior of particles under the influence of the external magnetic field and further utilization of the spherical Fe-Si particles in electrotechnical industry. The grain size and the crystallographic orientation of grains were analyzed by the electron backscattering diffraction (EBSD) technique.
2
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Advances in Powder Metallurgy Soft Magnetic Composite Materials

100%
Bureš R., Strečková M., Fáberová M., Kollár P., Füzer J.
Archives of Metallurgy and Materials
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2017
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vol. 62
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issue 2
3
Content available remote

FeSiBAlNiMo High Entropy Alloy Prepared by Mechanical Alloying

86%
Bureš R., Hadraba H., Fáberová M., Kollár P., Füzer J., Roupcová P., Strečková M.
Acta Physica Polonica A
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2017
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vol. 131
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issue 4
771-773
EN
High-entropy alloys have attracted increasing attentions because of their unique compositions, microstructures, and adjustable mechanical and functional properties. In this work, mechanical and magnetic properties of the FeSiBAlNiMo high-entropy alloy were studied in heat-treated conditions. Influence of temperature and time of sintering was investigated. The lowest coercivity H_c=370 A/m was reached at sintering temperature 580°C, during 20 min in Ar/10H₂ atmosphere. Resistivity decreases from R=0.006 Ωcm at 580°C of sintering temperature to R=0.0004 Ωcm at temperature 1100°C. Transverse rupture strength TRS = 340 MPa as well as the Young modulus E=87 GPa were much higher in the case of sintering at 1100°C in comparison to TRS = 5 MPa and E=7.5 GPa at sintering temperature 580°C. Low temperature consolidation made possible to structure recovery and stress relief of amorphous-nanocrystalline structure. Higher temperature above 1100°C induced sintering processes and formation of complex borides.
4
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Magnetic Properties of Soft Magnetic FeSi Composite Powder Cores

86%
Lauda M., Füzer J., Füzerová J., Kollár P., Strečková M., Fáberová M.
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vol. 126
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issue 1
144-145
EN
Soft magnetic composites (SMCs), which are used in electromagnetic applications, can be described as ferromagnetic powder particles surrounded by an electrical insulating film. These composite materials offer several advantages over traditional laminated steel cores such as reduction in weight and size. They have some unique properties, including three-dimensional isotropic ferromagnetic behaviour, very low eddy current loss, relatively low total core loss at medium and high frequencies, high electrical resistivity and good relative magnetic permeability. FeSi powder was used as a base ferromagnetic material for preparation of soft magnetic composites. The commercial FeSi particles of a precise spherical shape were prepared in two granulometric fractions (up to 150 μm or up to 356 μm). The phenol-formaldehyde resin modified by SiO_{2} nanoparticles was used as an electroinsulating layer. The FeSi particles covered by the synthesized resin were compacted at 800 MPa into the ring samples for magnetic measurements. The final samples were treated thermally under the curing schedule, which was suggested according to thermal degradation of the modified resin.
5
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Structure and Properties of Composites Based on Mixed Morphology of Ferromagnetic Particles

86%
Bureš R., Fáberová M., Strečková M., Birčáková Z., Kollár P., Füzer J.
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vol. 126
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issue 1
140-141
EN
Application potential of the soft magnetic composites increases with improvement of their functional properties. In addition to the magnetic properties, the mechanical properties of these materials are essential. The aim of this work was to investigate mechanical properties and their dependence on morphology of the ferromagnetic particles. Model composite based on Somaloy® and Vitroperm® powder was prepared using conventional powder metallurgy. The DC magnetic properties of composites based on two types of ferromagnetic particles with different shapes and structures are discussed in the relation with mechanical properties.
6
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The Influence of NiZnFe₂O₄ Content on Magnetic Properties of Supermalloy Type Material

73%
Ďáková L., Füzer J., Dobák S., Kollár P., Fáberová M., Strečková M., Bureš R., Hadraba H.
Acta Physica Polonica A
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2017
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vol. 131
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issue 4
813-815
EN
Soft magnetic composites represent a remarkable kind of materials with wide variety of use. Magnetic properties are dependent on the materials composition and also on the method of preparation. Ni-Fe-Mo alloys (supermalloy) have high complex permeability and low eddy current losses. Soft magnetic NiZnFe₂O₄ ferrites have low coercivity and intermediate saturation magnetization. The Ni_{80}Fe_{14.7}Mo_{4.5}Mn_{0.5}Si_{0.3} (wt%) powder sample was prepared by mechanical alloying of the chemical elements for 24 h. Ni_{0.3}Zn_{0.7}Fe₂O₄ ferrite is commercially available by Sigma Aldrich. Both powders were mixed at selected ratio and uniaxially compacted at 800 MPa. In this paper, we report the experimental observations of the effects of Ni_{0.3}Zn_{0.7}Fe₂O₄ content on the electromagnetic properties of NiFeMoMnSi/Ni_{0.3}Zn_{0.7}Fe₂O₄. The samples contained 5, 10, and 15% of Ni_{0.3}Zn_{0.7}Fe₂O₄ ferrite and were sintered for 30 min at 800°C. An addition of Ni_{0.3}Zn_{0.7}Fe₂O₄ ferrite caused decrease of complex permeability and increase coercivity of the samples. The 5% of Ni_{0.3}Zn_{0.7}Fe₂O₄ sample exhibits the highest value of the real part of complex permeability (48 at 1 kHz). The 10% of Ni_{0.3}Zn_{0.7}Fe₂O₄ sample showed the lowest total magnetic losses.
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