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Synthesis and characterization of coordination polymers prepared from CuII and NiII cyclam perchlorate and carmosine

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Vlassa M., Borodi G., Blăniţa G., Cojocaru I., Vlassa M., Silvestru C.
Open Chemistry
|
2011
|
vol. 9
|
issue 2
224-231
EN
Reaction of [CuII(cyclam)](ClO4)2 or [NiII(cyclam)](ClO4)2 in DMF with aqueous 4-hydroxy-3-(4-sulfonato-1-naphthylazo)naphthalen-1-sulfonate disodium salt (carmoisine) yielded coordination polymers {[CuII(cyclam)](carmoisine dianion)(H2O)5}n and powder {[NiII(cyclam)](carmoisine dianion)}n, respectively (cyclam = 1,4,8,11-tetrazacyclotetradecane). They were characterized by powder X-ray diffraction, IR, Raman spectrometry and TGA.
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