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EN
Changes in the phase composition and crystallite size, as well as changes in the magnetic behaviour of Nd_{4.5}Fe_{77}B_{18.5} alloy, caused by thermomagnetic measurements, was observed in regard of the optimal magnetic state of this alloy. In the optimized magnetic state, the formed nanocomposite consisted of Fe_3B/Nd_2Fe_{14}B and partly of α-Fe with a mean crystallite size < 30 nm, as determined by X-ray diffraction and transmission electron microscopy. An increased amount of α-Fe, the presence of Nd_2O_3 and different Fe-B phases, as well as an increase in the mean crystallite size were observed after thermomagnetic measurements had caused a quality loss of the hard magnetic properties.
EN
One of the more important developments in magnetic materials, polymer bonded magnets, have opened a new world of application opportunities. The Nd-Fe-B/polymer composite materials offer an excellent combination of strong magnetic and dynamical-mechanical properties. However, the transition temperatures of filler and matrix should be selected carefully considering the future application. Uniform particle distribution and good adhesion between Nd-Fe-B powder particles and polymer are essential for the quality of the composite, while stiffness of polymer matrix is one of the influencing factors as well. The damping properties of Nd-Fe-B/polymer composites with 15 wt.%, 50 wt.% and 75 wt.% of Nd-Fe-B powder were studied by dynamic mechanical analysis and compared with a pure polymer sample. Thermal stability was analyzed using a simultaneous differential scanning calorimetric and thermogravimetric analysis technique.
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