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Corrosion Behavior of Nitride and Cr-Al-N Coatings Formed on AISI D2 Steel

100%
Kılınc B., Demirkiran S., Sen U., Sen S.
Acta Physica Polonica A
|
2013
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vol. 123
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issue 2
268-270
EN
In the present work, the corrosion behavior of Cr-Al-N coating formed on the pre-nitrided AISI D2 cold work tool steel by thermo-reactive diffusion technique in the powder mixture consisting of ferro-chromium, aluminum, ammonium chloride and alumina at 1000C for 2 h was investigated. The phases formed in the coating layers were Cr_2N, (Cr,Fe)_2N_{1-x}, AlN, and Fe_2N which were confirmed by X-ray diffraction analysis. The uncoated, nitrided, and Cr-Al-N coated specimens were placed in corrosive media (3.5 wt% salt solution). A standard saturated calomel electrode was used as a reference and graphite as a counter or auxiliary electrode. The effectiveness of the coatings in preventing corrosion was tested in the NaCl solution by electrochemical impedance studies using the Nyquist plots and potentiodynamic studies as well. Conclusively, the application of nitride and Cr-Al-N layers on AISI D2 steel increased its surface hardness and corrosion resistance. The corrosion resistance of Cr-Al-N coatings is higher than that of uncoated and nitrided steels.
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Synthesis of Inconel 718 Superalloy by Electric Current Activated Sintering

88%
Ergin N., Ozdemir O., Demirkiran S., Sen S., Sen U.
Acta Physica Polonica A
|
2015
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vol. 127
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issue 4
1100-1102
EN
In the present study, the production of Inconel 718 nickel based superalloy was carried out in an electric current activated sintering in open air under a uniaxial pressure of 300 MPa using Al, Ni, Fe, Cr, Ti, Co, Fe-Nb and Fe-Mo powders. This alloy was heat treated, following the conventional treatment which consists of a 1 h solution treated at 980°C, followed by air cooling and double ageing, 8 h at 720°C, furnace cooling at 55°C/h down to 620°C and ageing for 8 h. Optical and SEM examinations showed a dense microstructure with low amount of porosity. XRD studies showed the existence of the γ and MC type carbide (M atom is a Nb, Ti combination) and δ phases. The relative density of sample measured according to Archimedes' principle was 93.7%, and the microhardness of sample was about 343.8 HV_{0.1}.
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