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The Evolution of Microstructure and Mechanical Properties of Al-Mn-Fe-Si Alloys During Isothermal Annealing

100%
Poková M., Zimina M., Cieslar M.
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EN
Recrystallization during isothermal annealing is studied in a twin-roll cast Al-Mn-Fe-Si alloy with Zr addition. Al₃Zr precipitates, which are known to improve the recrystallization resistance by exerting the Zener drag on migrating grain boundaries, form during heat treatment at 450°C. Materials with and without Al₃Zr precipitates are subjected to 4 passes of equal channel angular pressing at room temperature and a submicrometric grain size is achieved. In the course of isothermal annealing materials recrystallize at 400°C, 425°C and 450°C. The time required for recrystallization follows an Arrhenius equation. Recrystallization kinetics is similar independently of the presence of Al₃Zr precipitates. Precipitation of α-Al(Mn,Fe)Si particles is thought to increase the recrystallization resistance in the material without Al₃Zr.
2
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Recrystallization in Multilayer Al99.99/AlMg3 Laminates Prepared by Accumulative Roll-Bonding

88%
Cieslar M., Poková M., Zimina M., Veselý J., Bajer J.
Acta Physica Polonica A
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2015
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vol. 128
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issue 4
487-490
EN
Composite multilayer sheets from Al/AlMg3 with 32 alternating layers of Al and AlMg3 were prepared by accumulative roll-bonding and their thermal stability was studied. Recrystallized 2 mm thick sheets of a commercial twin-roll cast AlMg3 alloy and high purity Al99.99 served as input materials. Electrical resistivity measurements were used for the integral monitoring of solute atoms distribution during annealing. Light optical microscopy was employed for the direct grain-size determination and recrystallization description. Post-mortem electron microscopy observations were performed on as-prepared and annealed specimens and they were combined with in situ heating electron microscopy in order to explain the observed annealing effects. A broadening of Al layers during annealing was observed and related to diffusion of magnesium.
3
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The Study of the Behavior of Constrained Groove Pressed Magnesium Alloy after Heat Treatment

64%
Zimina M., Bohlen J., Letzig D., Kurz G., Poková M., Knapek M., Zrník J., Cieslar M.
Acta Physica Polonica A
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2015
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vol. 128
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issue 4
775-778
EN
In this work twin-roll cast AZ31 magnesium strip of thickness 5.6 mm was subjected to the heat treatment and further constrained groove pressing. A comparison of the microstructure and microhardness of as-cast, constrained groove pressed and annealed material was carried out. The twin-roll cast strip exhibits an inhomogeneous structure which is replaced by a finer and uniform recrystallized one after aging at 450°C for 10 h. A significant increase of the microhardness was observed accompanied by a pronounce grain refinement. Nevertheless, the distribution of the grain size is unequal along the specimen width. Thermal stability of the deformed structure during subsequent annealing was investigated. It was shown that higher annealing temperatures result in a formation of a more uniform recrystallized structure and in a significant drop of microhardness down to the values obtained for as-cast alloy.
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