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Comparison of Microstructural and Mechanical Properties of Hydroxyapatite-Al₂O₃ Composites with Commercial Inert Glass (CIG) Addition

100%

Bulut B., Demirkol N., Erkmen Z., Kayali E.

Acta Physica Polonica A

2015

vol. 127

issue 4

1094-1096

Hydroxyapatite (HA) is one of the most widely used biomaterials for orthopedic and dental applications. However, HA is a brittle and weak material and this constrains its orthopedic applications. There are several methods for the improvement of mechanical properties of the HA. One of these methods is to strengthen the HA material by a secondary phase (i.e polymer, metal or ceramics), to make a stronger composite material. Alumina (Al₂O₃) is a bioinert material, which has been widely investigated as a reinforcing agent for HA. The aim of this study is to compare the microstructural and mechanical properties of HA-Al₂O₃ composites with the addition of 5 and 10 wt.% of commercial inert glass (CIG). The grain samples were produced according to BS 7253 at 350 MPa. Then, they were sintered at temperatures between 1000-1300°C for 4 hours. The samples were also analyzed by SEM + EDS to determine microstructural properties, phase analysis was done by X-ray diffractometer (XRD), mechanical properties were measured by compression and hardness tests. Results show that HA-Al₂O₃ composites with addition of 5 and 10 wt.% CIG have reached high density values and high mechanical properties, such as compression strength and hardness at 1300°C. The compression strength and hardness of composites has increased with the increasing CIG content.

Nano-Bioceramic Synthesis from Tropical Sea Snail Shells (Tiger Cowrie - Cypraea Tigris) with Simple Chemical Treatment

64%

Şahin Y., Gündüz O., Bulut B., Özyeğin L., Gökçe H., Ağaoğulları D., Chou J., Kayalı E., Ben-Nissan B., Oktar F.

Acta Physica Polonica A

2015

vol. 127

issue 4

1055-1058

In this study several bioceramic materials (i.e. hydroxyapatite, whitlockite) were prepared by using chemical synthesis method from sea snail shells (Tiger Cowrie - Cypraea Tigris), originated from Pacific Ocean. Marine shells usually present aragonite-calcite structures and generally, complicated and pressurized equipment is necessary to convert these structures into bioceramics. Instead of using complicated systems, a basic ultrasonic equipment and simple chemical synthesis method was used in the process. DTA analysis was performed to calculate the required amount of H₃PO₄ solution in order to set the appropriate stoichiometric ratio of Ca/P equal to 1.667 for HA bioceramic or to 1.5 for β-TCP bioceramic in the titration. The prepared batches were sintered at 800°C and 400°C for hydroxyapatite (HA) and β-tri calcium phosphate (β-TCP) forms respectively. X-ray diffraction analysis, scanning electron microscopy (SEM) and infrared observations (FTIR) were implemented for both TCP and HA bioceramics. By applying the chemical synthesis with basic ultrasonic equipment, this study proposes a simple way of production for nano-HA /TCP powders from a natural marine sources.

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2 Acta Physica Polonica A

2 2015

2 Bulut B.

1 Ağaoğulları D.

1 Ben-Nissan B.

1 Chou J.

1 Demirkol N.

1 Erkmen Z.

1 Gökçe H.

1 Gündüz O.

1 Kayali E.

1 Kayalı E.

1 Oktar F.

1 Özyeğin L.

1 Şahin Y.

Search results

Comparison of Microstructural and Mechanical Properties of Hydroxyapatite-Al₂O₃ Composites with Commercial Inert Glass (CIG) Addition

Nano-Bioceramic Synthesis from Tropical Sea Snail Shells (Tiger Cowrie - Cypraea Tigris) with Simple Chemical Treatment