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The synthesis and the structure elucidation of N,O-diacetyl derivative of cyclic 3-hydroxymelatonin

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Siwicka A., Reiter R., Tian D., Wojtasiewicz K., Leniewski A., Maurin J., Błachut D., Czarnocki Z.

Open Chemistry

2004

vol. 2

issue 3

425-433

Melatonin was subjected to an oxidation to give 3-hydroxymelatonin. All spectroscopic data for this compound were collected. Ab initio calculations for both possible configurations were performed. X-ray data on N,O-diacetyl derivative of 3-hydroxymelatonin allowed the unambigous structure determination.

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1 Open Chemistry

1 2004

1 Błachut D.

1 Czarnocki Z.

1 Leniewski A.

1 Maurin J.

1 Reiter R.

1 Siwicka A.

1 Tian D.

1 Wojtasiewicz K.

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The synthesis and the structure elucidation of N,O-diacetyl derivative of cyclic 3-hydroxymelatonin