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2014 | 16 | 2 | 95-98

Article title

Precipitation of Calcium Carbonate in the Presence of Urea at 293 K and 343 K

Content

Title variants

Languages of publication

EN

Abstracts

EN
The results of the precipitation of calcium carbonate from a waste post-distillation liquid (DS) and a sodium bicarbonate saturated solution – both from the Solvay method – in the presence of urea are presented. The investigation was carried out at 293 K and 343 K. Reagent dosage times of 1, 5, 10, 20 and 30 min, and urea concentrations of 5, 6 and 10 mol/dm3 were applied. The granulometric composition, the values of bulk and packing densities and the absorptiveness sorption of water and paraffin oil from the obtained calcium carbonate were investigated.

Publisher

Year

Volume

16

Issue

2

Pages

95-98

Physical description

Dates

online
26 - 6 - 2014

Contributors

  • Nicolaus Copernicus University, Faculty of Chemistry, 7 Gagarin Street, 87-100 Toruń, Poland, e-mail: fiodor@chem.umk.pl
  • Nicolaus Copernicus University, Faculty of Chemistry, 7 Gagarin Street, 87-100 Toruń, Poland, e-mail: fiodor@chem.umk.pl

References

  • 1. Białowicz, K., Trypuć, M. & Kiełkowska, U. (2010). Precipitation of calcium carbonate from distillation residues and a filtrates from the Solvay process at 293 K. Part 1. Processing of concentrated solutions. Przem. Chem. 89 (1), 72–76.
  • 2. Białowicz, K. (2010). Precipitation of calcium carbonate from distillation residues and a filtrates from the solvay processat 293 K. Part 2. Processing of diluted solutions. Przem. Chem. 89 (1), 77–80.
  • 3. Trypuć, M. & Białowicz, K. (2010). Precipitation of calcium carbonate from post-distillation liguid and post-filtration liquid from Solvay process in the presence of CaCO3 crystals. Przem. Chem. 89 (10), 1357–1360.
  • 4. Trypuć, M. & Białowicz, K. (2011). CaCO3 production using liquid waste from Solvay method. J. Clean. Product. 19, 751–756. DOI: 10.1016/j.jclepro.2010.11.009.[Crossref]
  • 5. Białowicz, K. & Trypuć, M. (2011). Effect of Rosulf an L and Sulforokanol L225/1 on calcium carbonate properties. Przem. Chem. 90 (1), 148–152.
  • 6. Białowicz, K. & Trypuć, M. (2011). Infiuence of precipitation conditions on the CaCO3 properties obtained from after distillation liquid and post – filtration liquid of Solvay method at 313 K. Przem. Chem. 90 (8), 1604–1607.
  • 7. Mazurek, K. (2012). Studies on the optimum conditions for leaching the spent vanadium catalyst from metallurgical plants with sodium hydroxide solutions. Przem. Chem. 91 (2), 234–238.
  • 8. Mazurek, K. (2009). Research on the development of optimal parameters of potassium compounds leaching from spent catalysts used for oxidation of sulfur(IV) oxide. Przem. Chem. 88 (9), 1033–1036.
  • 9. Mazurek, K. & Trypuć, M. (2009). Recovery of the components of the spent vanadium catalyst with sulfuric(VI) acid solutions. Przem. Chem. 88 (11), 1248–1251.
  • 10. Mazurek, K. (2013). Recovery of vanadium, potassium and iron from a spent vanadium catalyst by oxalic acid solution leaching, precipitation and ion exchange processes. Hydrometallurgy 134–135, 26–31. DOI: 10.1016/j.hydromet.2013.01.011.[WoS][Crossref]
  • 11. Mazurek, K. (2012). Extraction of vanadium and potassium compounds from the spent vanadium catalyst from the metallurgical plant. Pol. J. Chem. Techn. 14 (2), 49–53. DOI: 10.2478/v10026-012-0070-9.[WoS][Crossref]
  • 12. Trypuć, M., Chałat, M., Mazurek K. (2006). Solubility investigations in the Na2SO4 + V2O5 + H2O system from 293 K to 323 K. J. Chem. Eng. Data 51 (2), 322–325. DOI: 10.1021/je050233b.[Crossref]
  • 13. Domka, L. (1979). Infiuence of experimental conditions on the physicochemical properties of precipitated calcium carbonate. UAM, Chemia 33, Poznań.
  • 14. Loy, J.E., Guo, J. & Severtson, S.J. (2004). Role of Adsorpion Fractionation in Determining the CaCO3 Scale Inhibition Performance of Polydisperse Sodium Polyacrylate. Ind. Eng. Chem. Res. 43, 1882–1887. DOI: 10.1021/ie034078a.[Crossref]
  • 15. Process for the preparation of calcium carbonate, particularly for pharmaceutical – UP – Nr 158 809 (UMK).
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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_pjct-2014-0037
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