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Number of results

Journal

2011 | 9 | 2 | 417-422

Article title

Synthesis and characteristics of nanocrystalline materials in Ti, B, C and N containing system

Content

Title variants

Languages of publication

EN

Abstracts

EN
In this work, the results of investigations of manufacturing ceramic materials on the basis of Ti, B, C and N containing systems are presented. The nanocrystalline ceramics were synthesized using a non-hydrolytic sol-gel method. The process was carried out in two stages. In the first low-temperature stage the precursor was obtained. The synthesis of ceramic phases, however, was conducted in the second high-temperature stage, in an argon atmosphere. Depending on the initial composition of the mixtures, the temperature and the time, the following products were obtained: TiCx, TiCxN1−x, TiB2 and B4C.The course of the process was investigated by thermogravimetric and differential scanning calorimetry methods (TG-DSC) coupled with mass spectrometry (MS). The solid state products were identified with use of X-ray diffraction (XRD). The size of the crystallites was estimated by the Scherrer method. The structure and morphology images of nanocrystalline powders were obtained using scanning electron microscopy (SEM) and transmission electron microscopy (TEM).

Keywords

Publisher

Journal

Year

Volume

9

Issue

2

Pages

417-422

Physical description

Dates

published
1 - 4 - 2011
online
20 - 2 - 2011

Contributors

  • Institute of Materials Science and Engineering, West Pomeranian University of Technology in Szczecin, Av. Piastow 19, 70-310, Szczecin, Poland
author
  • Institute of Materials Science and Engineering, West Pomeranian University of Technology in Szczecin, Av. Piastow 19, 70-310, Szczecin, Poland
  • Institute of Materials Science and Engineering, West Pomeranian University of Technology in Szczecin, Av. Piastow 19, 70-310, Szczecin, Poland
author
  • Institute of Materials Science and Engineering, West Pomeranian University of Technology in Szczecin, Av. Piastow 19, 70-310, Szczecin, Poland
  • Institute of Materials Science and Engineering, West Pomeranian University of Technology in Szczecin, Av. Piastow 19, 70-310, Szczecin, Poland

References

  • [1] V.J. Tennery, C.B. Finch, C.S. Yust, G. Clark, In: R.K. Viswanadham, D.J. Rowcliffe, J. Gurland (Eds.), Science of Hard Materials (Plenum Press, New York, 1983) 891
  • [2] V.I. Matkovich, G.V. Samsonov, P. Hagenmuller, T. Lundstrom, Boron and refractory borides (Springer-Verlag, New York, 1977) http://dx.doi.org/10.1007/978-3-642-66620-9[Crossref]
  • [3] M.K. Ferber, P.F. Becher, C.B. Finch, J. Am. Ceram. Soc. 66, C2 (1983) http://dx.doi.org/10.1111/j.1151-2916.1983.tb09974.x[Crossref]
  • [4] L. Axelbaum, Metall. Mater. Trans. B28, 1199 (1997)
  • [5] L.S. Sigl, K.A. Schwetz, U. Dworak, Int. J. Refract. Met. Hard Mater. 12, 95 (1994) http://dx.doi.org/10.1016/0263-4368(93)90020-G[Crossref]
  • [6] R. Telle, L. Sigl, K. Takagi, In: R. Riedel (Ed.), Handbook of Ceramic Hard Materials (Wiley-VCH, New York, 2003) 927
  • [7] D. Vallauri, I.C. Atias Adrian, A. Chrysanthou, J. Eur. Ceram. Soc. 28, 1697 (2008) http://dx.doi.org/10.1016/j.jeurceramsoc.2007.11.011[Crossref]
  • [8] X. Zhou, S. Zhang, M. Zhu, B. Chen, Int. J. Self Propag. High Temp. Synth. 7, 403 (1998)
  • [9] D. Brodkin, S. Kalidindi, M. Barsoum, A. Zavaliangos, J. Am. Ceram. Soc. 79, 1945 (1996) http://dx.doi.org/10.1111/j.1151-2916.1996.tb08017.x[Crossref]
  • [10] A.K. Khanra, Bull. Mater. Sci. 30, 93 (2007) http://dx.doi.org/10.1007/s12034-007-0016-7[Crossref]
  • [11] A. Alizadeh, E.T. Nassaj, N. Ehsani, J. Eur. Ceram. Soc. 24, 3277 (2004)
  • [12] A. Sinha, T. Mahata, B.P. Sharma, J. Nucl. Mater. 301, 165 (2002) http://dx.doi.org/10.1016/S0022-3115(02)00704-3[Crossref]
  • [13] L.Z. Pei, H.N. Xiao, J. Mater. Process. Technol. 209, 2122 (2009) http://dx.doi.org/10.1016/j.jmatprotec.2008.05.003[Crossref]
  • [14] A.J. Li, Y.H. Zhen, Q. Yin, L.P. Ma, Y.S. Yin, Ceram. Int. 32, 849 (2006) http://dx.doi.org/10.1016/j.ceramint.2005.05.022[Crossref]
  • [15] A. Gursoy, K. Ferhat, T. Servet, J. Eur. Ceram. Soc. 23, 1243 (2003) http://dx.doi.org/10.1016/S0955-2219(02)00304-7[Crossref]
  • [16] S.H. Kang, D.J. Kim, J. Eur. Ceram. Soc. 27, 715 (2007) http://dx.doi.org/10.1016/j.jeurceramsoc.2006.04.053[Crossref]
  • [17] L. Shi et al., Solid State Commun. 1, 5 (2003) http://dx.doi.org/10.1016/S0038-1098(03)00627-6[Crossref]
  • [18] A. Biedunkiewicz, J. Sol-GelSci. Technol. (in press)
  • [19] A. Biedunkiewicz, M. Wysiecki, P. Noworol, Polish Patent P200978 (2008)
  • [20] J.I. Langford, A.J.C. Wilson, J. Appl. Crystallogr. 11, 102 (1978) http://dx.doi.org/10.1107/S0021889878012844[Crossref]
  • [21] A.S. Kurlo, A.I. Guse, Glass Phys. Chem. 33, 276 (2007) http://dx.doi.org/10.1134/S1087659607030169[Crossref]
  • [22] A. Biedunkiewicz, P. Figiel, M. Sabara, Mater. Sci. (in press)

Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11534-010-0121-x
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