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Journal

2006 | 4 | 4 | 604-619

Article title

Novel soluble aromatic poly(amideimide)s containing 9,9-diphenylfluorene moieties: characterization and optical properties

Content

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Languages of publication

EN

Abstracts

EN
A series of aromatic poly(amideimide)s containing 9,9-diphenylfluorene moieties and the amide units in the main chain have been synthesized by solution polycondensation reaction of newly prepared diamidedianhydride with several aromatic diamines: 1,3-phenylenediamine, 3,3′-dimethoxy-biphenyl-4,4′-diamine, 4,4′-oxydianiline, 4,4′-(1,3-phenylenedioxy)dianiline, 4,4′-(9-fluorenylidene)dianiline and 1,5-diaminonaphthalene. Molecular structures of the polymers obtained have been characterized using 13C NMR, 1H NMR and FTIR spectroscopies. The polymers prepared are readily soluble in aprotic polar solvents, and form optically transparent films by solution casting. The resultant poly(amideimide)s have been analyzed by differential scanning calorimetry (DSC), thermogravimetry (TG) and wide-angle X-ray diffraction measurements. They exhibited high levels of thermal stability, with decomposition temperatures in the range 452–494 °C, and high glass transition temperatures (181–278 °C). The optical behavior of these polymers has been investigated in NMP solution as well as in the films. The photoluminescence (PL) spectra of the free-standing films prepared from the poly(amideimide)s exhibited maximum emission bands around 506–525 nm in the green region.

Publisher

Journal

Year

Volume

4

Issue

4

Pages

604-619

Physical description

Dates

published
1 - 12 - 2006
online
1 - 12 - 2006

Contributors

  • Centre of Polymer Chemistry, Polish Academy of Sciences, 41-819, Zabrze, Poland
  • Centre of Polymer Chemistry, Polish Academy of Sciences, 41-819, Zabrze, Poland
  • Centre of Polymer Chemistry, Polish Academy of Sciences, 41-819, Zabrze, Poland
  • Centre of Polymer Chemistry, Polish Academy of Sciences, 41-819, Zabrze, Poland
  • Paint & Plastics Department in Gliwice, Institute for Plastics Processing METALCHEM, 44-100, Gliwice, Poland
  • Centre of Polymer Chemistry, Polish Academy of Sciences, 41-819, Zabrze, Poland

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Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-006-0029-x
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