PL EN


Preferences help
enabled [disable] Abstract
Number of results
1997 | 91 | 5 | 961-968
Article title

Optimization of Azimuthal Scan Procedure for Absolute Structure Determination

Content
Title variants
Languages of publication
EN
Abstracts
EN
The paper describes the application of the azimuthal scan technique for absolute structure determination using X-ray anomalous dispersion. A diffraction pattern with rotation around the scattering vector provides information about various anisotropic effects: absorption, extinction and multi-beam interaction. Recording of azimuthal scans for Friedel pairs is proposed as an alternative to single reflection measurement. Several factors affecting the smoothness of the azimuthal scan curves are discussed and a procedure for eliminating various sources of errors, involving a Fourier filtering, is proposed in order to increase feasibility of chiral discrimination.
Keywords
EN
Publisher

Year
Volume
91
Issue
5
Pages
961-968
Physical description
Dates
published
1997-05
Contributors
author
  • Regional Laboratory of Physicochemical Analysis and Structural Research, Jagiellonian University, Ingardena 3, 30-060 Kraków, Poland
author
  • Regional Laboratory of Physicochemical Analysis and Structural Research, Jagiellonian University, Ingardena 3, 30-060 Kraków, Poland
References
Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.bwnjournal-article-appv91z521kz
JavaScript is turned off in your web browser. Turn it on to take full advantage of this site, then refresh the page.