Phase Structure and Heat Generation in the Co-Precipitated Magnetite Nanoparticles

• Authors: P. Pawlik , M. Pruba , K. Pawlik , K. Kotynia
• Languages of publication: EN

Abstracts

EN

In the present studies the phase structure and magnetic ordering of magnetite nanoparticles were investigated. The powder samples were obtained by co-precipitation from Fe(III) and Fe(II) salts. SiO₂ coating was performed using the modified Stöber process. X-ray diffraction studies revealed presence of the only one Fe₃O₄ crystalline phase both for the non-coated and SiO₂-coated samples. The Mössbauer studies have shown differences in shapes of measured spectral lines for Fe₃O₄ particles subjected to the Stöber process and non-coated particles. The heating efficiency was measured for glycerol dispersed nanoparticles. The analysis have shown changes in specific loss power depending on the concentration of the nanoparticles and amplitude of alternating magnetic field.

Keywords

EN

75.47.Lx; 78.67.Bf; 78.70.Ck; 76.80.+y; 87.50.S-

Discipline

• 78.67.Bf: Nanocrystals, nanoparticles, and nanoclusters
• 76.80.+y: Mössbauer effect; other γ-ray spectroscopy(see also 33.45.+x Mössbauer spectra—in atomic and molecular physics; for biophysical applications, see 87.64.kx; for chemical analysis applications, see 82.80.Ej)
• 75.47.Lx: Magnetic oxides
• 78.70.Ck: X-ray scattering
• 87.50.S-: Radiofrequency/microwave fields effects

• Publisher: Institute of Physics, Polish Academy of Sciences
• Journal: Acta Physica Polonica A
• Year: 2017
• Volume: 131
• Issue: 5
• Pages: 1217-1221

Dates

published

2017-05

Contributors

author

P. Pawlik

• Institute of Physics, Częstochowa University of Technology, al. Armii Krajowej 19, 42-200 Częstochowa, Poland

author

M. Pruba

• Institute of Physics, Częstochowa University of Technology, al. Armii Krajowej 19, 42-200 Częstochowa, Poland

author

K. Pawlik

• Institute of Physics, Częstochowa University of Technology, al. Armii Krajowej 19, 42-200 Częstochowa, Poland

author

K. Kotynia

• Institute of Physics, Częstochowa University of Technology, al. Armii Krajowej 19, 42-200 Częstochowa, Poland

References

• [1] B.N. Ames, L. Swirsky Gold, Mutat. Res./Fundament. Mol. Mech. Mutagen. 447, 3 (2000), doi: 10.1016/S0027-5107(99)00194-3
• [2] V.T. DeVita Jr., S. Hellman, S.A. Rosenberg, Cancer Principles and Practice of Oncology, 7th ed., Lippincott Williams & Wilkins, Philadelphia 2005
• [3] F. Roila, P.J. Hesketh, J. Herrstedt, Ann. Oncol. 17, 20 (2006), doi: 10.1093/annonc/mdj078
• [4] A. Skumiel, M. Izydorzak, M. Leonowicz, A.D. Pomogailo, G.I. Dzhardimalieva, Int. J. Thermophys. 32, 1973 (2011), doi: 10.1007/s10765-011-1029-4
• [5] M. Izydorzak-Wozniak, M. Leonowicz, J. Nanosci. Nanotechnol. 14, 2258 (2014), doi: 10.1166/jnn.2014.8516
• [6] H. Chiriac, T. Petreus, E. Carasevici, L. Labusca, D. Herea, C. Danceanu, N. Lupu, J. Magn. Magn. Mater. 380, 13 (2015), doi: 10.1016/j.jmmm.2014.10.015
• [7] S. Dutz, R. Hergt, Nanotechnology 25, 452001 (2014), doi: 10.1088/0957-4484/25/45/452001
• [8] A. Brezovich, in: Med. Phys. Monograph, American Institute of Physics, New York 1988, p. 82
• [9] Q.A. Pankhurst, J. Connolly, S.K. Jones, J. Dobson, J. Phys. D Appl. Phys. 36, 167 (2003), doi: 10.1088/0022-3727/36/13/201
• [10] Y.H. Deng, D.W. Qi, C.H. Deng, X.M. Zhang, D.Y. Zhao, J. Am. Chem. Soc. 130, 28 (2008), doi: 10.1021/ja0777584
• [11] M.A. Ghasemzadeh, Acta Chim. Slov. 62, 977 (2015), doi: 10.17344/acsi.2015.1501
• [12] I. Smolkova, N. Kazantseva, V. Babayan, P. Smolka, H. Parmar, J. Vilcakova, O. Schneeweiss, N. Pizurova, J. Magn. Magn. Mater. 374, 508 (2015), doi: 10.1016/j.jmmm.2014.08.096
• [13] I.S. Smolkova, N.E. Kazantseva, H. Parmar, V. Babayan, P. Smolka, P. Saha, Mater. Chem. Phys. 155, 178 (2015), doi: 10.1016/j.matchemphys.2015.02.022
• [14] A. Demir, A. Baykal, H. Sozeri, R. Topkaya, Synth. Met. 187, 75 (2014), doi: 10.1016/j.synthmet.2013.10.027
• [15] A. Mitra, J. Mohapatra, S.S. Meena, C.V. Tomy, M. Aslam, J. Phys. Chem. C 118, 19356 (2014), doi: 10.1021/jp501652e
• [16] B. Kalska-Szostko, M. Zubowska, D. Satuła, Acta Phys. Pol. A 109, 365 (2006), doi: 10.12693/APhysPolA.109.365
• [17] A. Jordan, P. Wust, H. Fahling, W. John, A. Hinz, R. Felix, Int. J. Hyperther. 25, 499 (2009), doi: 10.3109/02656730903287790
• [18] S. Laurent, S. Dutz, U.O. Hafeli, M. Mahmoudi, Adv. Coll. Interf. 166, 8e23 (2011), doi: 10.1016/j.cis.2011.04.003
• [19] A. Figuerola, R. Di Corato, L. Manna, T. Pellegrino, Pharmacol. Res. 62, 126 (2010), doi: 10.1016/j.phrs.2009.12.012

Identifiers

DOI

10.12693/APhysPolA.131.1217