A System of B-C-N-O: Synthesis, Characterization and Determination of Unit Cell Parameters

• Authors: G. Gül , F. Kurtuluş
• Languages of publication: EN

Abstracts

EN

Boron-rich solids are good candidates to apply instead of diamond. Boron has a unique crystal structure and compounds of it are resistant to heat treatment. These structures have light density, high hardness, and chemically inertness. Also, boron compounds display thermal and electronic properties as a thermoelectric power at high temperatures. A boron, carbon, nitrogen, and oxygen containing compound was synthesized for the first time by classical microwave method using elemental amorphous boron, active carbon, and urea with 1:1:1 molar ratio. The compound is crystallized in monoclinic system with unit cell parameters a=12.9575 Å, b=9.3264 Å, c=9.6529 Å, β =113.277° which are calculated by POWD indexing program. The X-ray diffraction, POWD, the Fourier transform infrared, scanning electron microscopy/energy X-ray diffraction spectroscopy and thermogravimetric/different thermal analysis were achieved.

Keywords

EN

33.20.Ea; 61.66.-f; 61.66.Fn; 84.40.-x

Discipline

• 61.66.Fn: Inorganic compounds
• 84.40.-x: Radiowave and microwave (including millimeter wave) technology(for microwave, submillimeter wave, and radiowave receivers and detectors, see 07.57.Kp; for microwave and radiowave spectrometers, see 07.57.Pt; for radiowave propagation, see 41.20.Jb)
• 61.66.-f: Structure of specific crystalline solids(for surface structure, see 68.35.B-)
• 33.20.Ea: Infrared spectra

• Publisher: Institute of Physics, Polish Academy of Sciences
• Journal: Acta Physica Polonica A
• Year: 2017
• Volume: 131
• Issue: 1
• Pages: 36-38

Dates

published

2017-01

Contributors

author

G. Gül

• Balıkesir University, Department of Chemistry, 10145 Balıkesir, Turkey

author

F. Kurtuluş

• Balıkesir University, Department of Chemistry, 10145 Balıkesir, Turkey

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Identifiers

DOI

10.12693/APhysPolA.131.36