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A nanopowder containing γ-Fe₂O₃ particles was synthesized by adding a gas mixture of H₂/Fe(CO)₅ into a microwave torch discharge at 1 bar. The presence of γ-Fe₂O₃ phase was confirmed by powder X-ray diffraction (mean crystallite size d_{XRD}=24 nm). The dominating characteristic sextets of γ-Fe₂O₃ were identified in the Mössbauer spectrum taken at 5 K. The presence of pure Fe₃O_4 in the nanopowder was excluded. The Mössbauer spectrum taken at 5 K exhibited six times larger total spectrum area than the Mössbauer spectrum taken at 293 K. Zero field cooled/field cooled curves measured down to 4 K in the magnetic field of 7.9 kA/m are reported.
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168
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published
2016-01
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Publication order reference
YADDA identifier
bwmeta1.element.bwnjournal-article-appv129n1p32kz
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