Preparation of Carbon Nanomaterials over Ni/ZSM-5 Catalyst Using Simplex Method Algorithm

• Authors: J. Majewska , B. Michalkiewicz
• Languages of publication: EN

Abstracts

EN

Carbon nanomaterials were prepared from methane by catalytic decomposition over a nickel-supported ZSM-5 catalyst. The mole ratio of SiO₂ to Al₂O₃ in ZSM-5 was 200-400. The nickel content was varied from 17 to 23 wt% Ni. In order to find the greatest yield and the highest quality of carbon nanomaterials the simplex design method for planning the experiments was applied. Different parameters such as: temperature, methane flow, nitrogen flow and nickel content in the catalyst were evaluated. The carbon nanomaterials were analyzed by the Raman spectroscopy, scanning and transmission electron microscopy, and total organic carbon analyzer.

Keywords

EN

81.07.De; 81.16.Hc; 81.15.Gh

Discipline

• 81.07.De: Nanotubes
• 81.16.Hc: Catalytic methods
• 81.15.Gh: Chemical vapor deposition (including plasma-enhanced CVD, MOCVD, ALD, etc.)(for chemistry of MOCVD, see 82.33.Ya in physical chemistry and chemical physics)

• Journal: Acta Physica Polonica A
• Year: 2016
• Volume: 129
• Issue: 1
• Pages: 153-157

Dates

published

2016-01

received

2015-07-05

(unknown)

2015-12-09

Contributors

author

J. Majewska

• West Pomeranian University of Technology in Szczecin, K. Pułaskiego 10, 70-322 Szczecin, Poland

author

B. Michalkiewicz

• West Pomeranian University of Technology in Szczecin, K. Pułaskiego 10, 70-322 Szczecin, Poland

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Identifiers

DOI

10.12693/APhysPolA.129.153