Nano-Bioceramic Synthesis from Tropical Sea Snail Shells (Tiger Cowrie - Cypraea Tigris) with Simple Chemical Treatment

• Authors: Y. Şahin , O. Gündüz , B. Bulut , L. Özyeğin , H. Gökçe , D. Ağaoğulları , J. Chou , E. Kayalı , B. Ben-Nissan , F. Oktar
• Languages of publication: EN

Abstracts

EN

In this study several bioceramic materials (i.e. hydroxyapatite, whitlockite) were prepared by using chemical synthesis method from sea snail shells (Tiger Cowrie - Cypraea Tigris), originated from Pacific Ocean. Marine shells usually present aragonite-calcite structures and generally, complicated and pressurized equipment is necessary to convert these structures into bioceramics. Instead of using complicated systems, a basic ultrasonic equipment and simple chemical synthesis method was used in the process. DTA analysis was performed to calculate the required amount of H₃PO₄ solution in order to set the appropriate stoichiometric ratio of Ca/P equal to 1.667 for HA bioceramic or to 1.5 for β-TCP bioceramic in the titration. The prepared batches were sintered at 800°C and 400°C for hydroxyapatite (HA) and β-tri calcium phosphate (β-TCP) forms respectively. X-ray diffraction analysis, scanning electron microscopy (SEM) and infrared observations (FTIR) were implemented for both TCP and HA bioceramics. By applying the chemical synthesis with basic ultrasonic equipment, this study proposes a simple way of production for nano-HA /TCP powders from a natural marine sources.

Keywords

EN

81.07.-b; 87.68.+z; 28.52.Fa

Discipline

• 28.52.Fa: Materials
• 81.07.-b: Nanoscale materials and structures: fabrication and characterization(for structure of nanoscale materials, see 61.46.-w; for nanostructured materials in electrochemistry, see 82.45.Yz; see also 62.23.-c Structural classes of nanoscale systems in mechanical properties of condensed matter)

• Publisher: Institute of Physics, Polish Academy of Sciences
• Journal: Acta Physica Polonica A
• Year: 2015
• Volume: 127
• Issue: 4
• Pages: 1055-1058

Dates

published

2015-04

Contributors

author

Y. Şahin

• Department of Biomedical Engineering, Faculty of Engineering and Architecture, Istanbul Arel University, Istanbul, Turkey

author

O. Gündüz

• Department of Metallurgy and Materials Engineering, Faculty of Technology, Marmara University, Istanbul, Turkey
• Applied and Research Centre for Nanotechnology and Biomaterials, Marmara University, Istanbul, Turkey

author

B. Bulut

• Metallurgical and Materials Engineering Department, Istanbul Technical University, Istanbul, Turkey

author

L. Özyeğin

• Bayramoglu, Kocaeli, Turkey

author

H. Gökçe

• Metallurgical and Materials Engineering Department, Istanbul Technical University, Istanbul, Turkey
• Prof. Dr. Adnan Tekin Materials Scienci and Production Technology Applied Research Center, Istanbul Technical University, Istanbul, Turkey

author

D. Ağaoğulları

• Metallurgical and Materials Engineering Department, Istanbul Technical University, Istanbul, Turkey

author

J. Chou

• Research Institute of Pharmaceutical Sciences, Musashino University, Tokyo, Japan

author

E. Kayalı

• Metallurgical and Materials Engineering Department, Istanbul Technical University, Istanbul, Turkey

author

B. Ben-Nissan

• Department of Chemistry and Forensic Sciences, The University of Technology, Sydney, Australia

author

F. Oktar

• Bioengineering Department, Faculty of Engineering Marmara University, Istanbul, Turkey
• Applied and Research Centre for Nanotechnology and Biomaterials, Marmara University, Istanbul, Turkey

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Identifiers

DOI

10.12693/APhysPolA.127.1055