The Effect of Temperature on Grain Size of SnO_2 Nanoparticles Synthesized by Sol-Gel Method

• Authors: H. Köse , A. Aydin , H. Akbulut
• Languages of publication: EN

Abstracts

EN

Tin dioxide nanoparticles were synthesized by sol-gel method and calcined at different temperatures in the range 350-750°C. The SnO_2 precursor solution was prepared from SnCl_2 ·2H_2O (tin (II) chloride dihydrate), and chloride ions were removed from the solution before the sol-gel synthesis was applied. SnO_2 powders were characterized by thermal analyses, X-ray diffraction, field emission gun-scanning electron microscopy, and energy dispersive X-ray spectroscopy, and grain size of nanoparticles were determined by using the Debye-Scherrer formula.

Keywords

EN

81.07.Wx; 81.20.Fw; 81.20.Ev

Discipline

• 81.07.Wx: Nanopowders
• 81.20.Ev: Powder processing: powder metallurgy, compaction, sintering, mechanical alloying, and granulation
• 81.20.Fw: Sol-gel processing, precipitation(for reactions in sol-gels, see 82.33.Ln; for sol-gels as disperse system, see 82.70.Gg)

• Publisher: Institute of Physics, Polish Academy of Sciences
• Journal: Acta Physica Polonica A
• Year: 2014
• Volume: 125
• Issue: 2
• Pages: 345-347

Dates

published

2014-02

Contributors

author

H. Köse

• Department of Chemistry, Arts and Sciences Faculty, Sakarya University, 54187, Sakarya, Turkey

author

A. Aydin

• Department of Chemistry, Arts and Sciences Faculty, Sakarya University, 54187, Sakarya, Turkey

author

H. Akbulut

• Department of Metallurgy and Material Engineering, Engineering Faculty, Sakarya University, 54187, Sakarya, Turkey

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Identifiers

DOI

10.12693/APhysPolA.125.345