EN
Seleno-spinels with nominal chemical composition Cu_{0.5}Fe_{0.5}Cr_2Se_4 and Cu_{0.2}Fe_{0.8}Cr_2Se_4 were prepared as polycrystalline samples using ceramic method. The assumed composition was verified by wavelength-dispersive X-ray fluorescence spectrometry. The X-ray analysis was carried out in order to make phase analysis and to compare its results with those obtained with the Mössbauer spectroscopy.