Mn₂O₃ Nanoparticles Synthesized from Thermal Decomposition of Manganese(II) Schiff Base Complexes

• Authors: A. Khalaji , M. Ghorbani
• Languages of publication: EN

Abstracts

EN

The Mn₂O₃ nanoparticles have been prepared using solid state thermal decomposition of MnL¹ and MnL², L¹=N,N'-bis(2-hydroxy-4-methoxybenzophenone)-1,3-propanediamine and L²=N,N'-bis(2-hydroxy-4-methoxybenzophenone)-1,2-cyclohexanediamine, at 500°C for 3 h and characterized by the Fourier transform infrared spectroscopy, X-ray powder diffraction and scanning electron microscopy. The Fourier transform infrared spectroscopy and X-ray powder diffraction confirm that the formed product at 500°C is Mn₂O₃. The MnL¹ and MnL² complexes were prepared from the one-pot reaction of MnCl₂·H₂O, diamine and 2-hydroxy-4-methoxybenzophenone and characterized by elemental analyses, the Fourier transform infrared spectroscopy and thermogravimetry.

Keywords

EN

Mn₂O₃ nanoparticles; manganese(II); Schiff base; thermal decomposition

• Publisher: Institute of Physics, Polish Academy of Sciences
• Journal: Acta Physica Polonica A
• Year: 2018
• Volume: 133
• Issue: 1
• Pages: 7-9

Dates

published

2018-01

received

2017-05-14

(unknown)

2017-10-04

Contributors

author

A. Khalaji

• Department of Chemistry, Faculty of Science, Golestan University, Gorgan, Iran

author

M. Ghorbani

• Department of Chemistry, Payame Noor University, P.O. Box 19395-3697, Tehran, Iran

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Identifiers

DOI

10.12693/APhysPolA.131.7