The results of the studies of bis(1-chloro-2-propyl) ether adsorption from aqueous solution onto AG5 activated carbon were presented here. Dynamic adsorptivity, mass transfer zone and the velocity of the adsorption front of the 10cm adsorption bed depth for the velocity of flow 9 and 25 cm/min were determined. For the regeneration of the adsorption bed, acetone rinsing was used. Total washout of adsorbed bis(1-chloro-2-propyl) ether from the bed was obtained. After the regeneration the adsorbent has not shown deterioration of adsorption properties. To isolate bis(1-chloro-2-propyl) ether from acetone, distillation was used.