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2013 | 1 | 38-53
Article title

Microextraction using packed sorbent as an effective and
high-throughput sample extraction technique: Recent
applications and future trends.

Content
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Languages of publication
EN
Abstracts
EN
In the last decade, several developments, particularly in the liquid
chromatography and hyphenated techniques fields, have allowed
researchers to reach analytical limits that are becoming very close to the
single molecule level. Sample preparation, however, despite being a key
step in the analytical methodology, did not track these developments
and very few approaches able to cope with these stringent analytical
requirements were developed. One such approach is microextraction by
packed sorbent (MEPS), a sophisticated and miniaturized form of solid
phase extraction that has reduced to the microliter scale every step of
the sample extraction methodology including sample volume and solvent
usage. Simultaneously, the amount of extraction phase used was also
reduced and, more importantly, the sorbent is reusable dozens of times
which significantly lowers the cost of analysis versus other solid-phase
extraction approaches. In this review, we will update the state-of-the-art
of the MEPS technique, focusing on the trends and applications reported
since 2010 and future perspectives and developments that in our view
will further improve the high-throughput potential and applications of this
sample preparation methodology.
Publisher

Year
Volume
1
Pages
38-53
Physical description
Dates
accepted
02 - 08 - 2013
received
15 - 03 - 2013
online
30 - 10 - 2013
Contributors
author
  • CQM - Centro de Química da Madeira,
    Universidade da Madeira, Centro de
    Ciências Exatas e da Engenharia da
    Universidade da Madeira, Campus
    Universitário da Penteada, 9000-390
    Funchal, Portugal, jamp@uma.pt
author
  • CQM - Centro de Química da Madeira,
    Universidade da Madeira, Centro de
    Ciências Exatas e da Engenharia da
    Universidade da Madeira, Campus
    Universitário da Penteada, 9000-390
    Funchal, Portugal
author
  • CQM - Centro de Química da Madeira,
    Universidade da Madeira, Centro de
    Ciências Exatas e da Engenharia da
    Universidade da Madeira, Campus
    Universitário da Penteada, 9000-390
    Funchal, Portugal
author
  • CQM - Centro de Química da Madeira,
    Universidade da Madeira, Centro de
    Ciências Exatas e da Engenharia da
    Universidade da Madeira, Campus
    Universitário da Penteada, 9000-390
    Funchal, Portugal
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Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_sampre-2013-0005
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