Carbon nanotube-ionic liquid nanocomposite modified carbon-ceramic electrode for determination of dopamine in real samples

• Authors: Mir Majidi , Reza Baj , Abdolhossein Naseri
• Languages of publication: EN

Abstracts

EN

Room temperature 1-butyl-3-methylimidazolium tetraflouroborate ([BMIM][BF4]) ionic liquid was employed for dispersion of multi walled carbon nanotubes (MWCNTs) and the formation of nanocomposite on the surface of a carbon-ceramic electrode. The surface of the modified electrode was characterized using scanning electron microscopy and electrochemical impedance spectroscopy. The modified electrode exhibited excellent electrochemical activity to oxidation of dopamine (DA); whereas electro oxidation of ascorbic acid (AA) was not seen and electro oxidation of uric acid (UA) appeared at a more positive potential than DA. The multi walled carbon nanotube-ionic liquid nanocomposite modified carbon-ceramic electrode was used for the selective determination of DA in the presence of high levels of AA and UA using differential pulse voltammetry. The calibration curve for DA was linear in the range of 3.00 to 130 µM with the detection limit (S/N=3) of 0.87 µM. The present electrode was successfully applied to the determination of DA in some commercial pharmaceutical samples and human blood serum. [...]

Keywords

EN

Multi walled carbon nanotubes; Ionic liquid; Nanocomposite; Dopamine; Carbon-ceramic electrode

• Publisher: De Gruyter Open
• Journal: Open Chemistry
• Year: 2013
• Volume: 11
• Issue: 7
• Pages: 1172-1186

Dates

published

1 - 7 - 2013

online

26 - 4 - 2013

Contributors

author

Mir Majidi

• Department of Analytical Chemistry, Faculty of Chemistry, University of Tabriz, Tabriz, 51664, Iran

author

Reza Baj

• Department of Analytical Chemistry, Faculty of Chemistry, University of Tabriz, Tabriz, 51664, Iran

author

Abdolhossein Naseri

• Department of Analytical Chemistry, Faculty of Chemistry, University of Tabriz, Tabriz, 51664, Iran

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Identifiers

DOI

10.2478/s11532-013-0251-2