PL EN


Preferences help
enabled [disable] Abstract
Number of results
Journal
2011 | 9 | 1 | 133-142
Article title

Development of a rapid resolution HPLC method for the separation and determination of 17 phenolic compounds in crude plant extracts

Content
Title variants
Languages of publication
EN
Abstracts
EN
Rapid Resolution HPLC/DAD method, on a 1.8 µm, 4.6×50 mm column, was developed to enable a rapid separation of a mixture of 17 compounds, which consisted of hydroxybenzoic acids, hydroxycinnamic acids, flavones, flavonols, flavanone, flavonol-glycoside and antraquinone, in a single run, within 22 minutes. The developed method is precise, accurate and sensitive enough for simultaneous quantitative evaluation of major compounds in crude and hydrolyzed extracts of parsley, buckthorn, mint, caraway and birch. In order to overcome the inability to quantify all the phenolic compounds present in the samples caused by lack of external standards, HPLC approaches for the total phenolic content estimation based on sum of all integrated peak areas were made. These results were compared with the total phenolic content determined by Folin-Cioacalteu method. Although the correlation between the series of data was not significant (pHPLC was not high in the case of parsley, buckthorn and mint extract. Regarding the obtained results, the HPLC approach could serve as an excellent tool for total phenolic content estimation, without the need for complete identification of the individual compounds. [...]
Publisher
Journal
Year
Volume
9
Issue
1
Pages
133-142
Physical description
Dates
published
1 - 2 - 2011
online
16 - 12 - 2010
References
  • [1] K. Herrmann, J. Food Technol. 11, 433 (1976) http://dx.doi.org/10.1111/j.1365-2621.1976.tb00743.x[Crossref]
  • [2] E. Wollenweber, V.H. Dietz, Phytochemistry 20, 869 (1981) http://dx.doi.org/10.1016/0031-9422(81)83001-4[Crossref]
  • [3] R.W. Hemingway, P.E. Laks, Plant Polyphenols: Synthesis, Properties, Significance, (Kluwer Academic/Plenum, New York, 1992) 264
  • [4] V.L. Singleton, R. Orthofer, R.M. Lamuela-Raventos, Methods Enzymol. 299, 152 (1999) http://dx.doi.org/10.1016/S0076-6879(99)99017-1[Crossref]
  • [5] J.M. Harnly, R.F. Doherty, G.R. Beecher, J.M. Holden, D.B. Haytowitz, S. Bhagwat, S. Gebhardt, J. Agric. Food Chem. 54, 9966 (2006) http://dx.doi.org/10.1021/jf061478a[Crossref]
  • [6] I. Molnár-Perl, Z. Füzfai, J. Chromatogr. A 1073, 201 (2005) http://dx.doi.org/10.1016/j.chroma.2004.10.068[Crossref]
  • [7] H.M. Merken, G.R. Beecher, J. Chromatogr. A 897, 177 (2000) http://dx.doi.org/10.1016/S0021-9673(00)00826-8[Crossref]
  • [8] H. Sakakibara, Y. Honda, S. Nakagawa, H. Ashida, K. Kanazawa, J. Agric. Food Chem. 51, 571 (2003) http://dx.doi.org/10.1021/jf020926l[Crossref]
  • [9] D. Guillarme, D.T.-T. Nguye, S. Rudaz, J.-L. Veuthey, J. Chromatogr. A 1149, 20 (2007) http://dx.doi.org/10.1016/j.chroma.2006.11.014[Crossref]
  • [10] U. Justesen, P. Knuthsen, T. Leth, J. Chromatogr. A 799, 101 (1998) http://dx.doi.org/10.1016/S0021-9673(97)01061-3[Crossref]
  • [11] M. Krizman, D. Baricevic, M. Prosek, J. Pharm. Biomed. Anal. 43, 481 (2007) http://dx.doi.org/10.1016/j.jpba.2006.07.029[Crossref]
  • [12] K. Dallenbach-Tölke, Sz. Nyiredy, B. Meier, O. Sticher, Planta Med. 53, 189 (1987) http://dx.doi.org/10.1055/s-2006-962669[Crossref]
  • [13] V. Ossipov, K. Nurmi, J. Loponen, E. Haukioja, K. Pihlaja, J. Chromatogr. A 721, 59 (1996) http://dx.doi.org/10.1016/0021-9673(95)00765-2[Crossref]
  • [14] B. Voirin, C. Bayet, O. Faure, F. Jullien, Phytochemistry 50, 1189 (1999) http://dx.doi.org/10.1016/S0031-9422(98)00672-4[Crossref]
  • [15] X.Y. Gao, Y. Jiang, J. Lu, P.F. Tu, J. Chromatogr. A 1216, 2118 (2009) http://dx.doi.org/10.1016/j.chroma.2008.11.104[Crossref]
  • [16] D.J. Guédon, B.P. Pasquier, J. Agric. Food Chem. 42, 679 (1994) http://dx.doi.org/10.1021/jf00039a015[Crossref]
  • [17] K. Triantaphyllou, G. Blekas, D. Boskou, Int. J. Food Sci. Nutr. 52, 313 (2001) http://dx.doi.org/10.1080/09637480120057512[Crossref]
  • [18] F.M. Areias, P. Valentão, P.B. Andrade, F. Ferreres, R.M. Seabra, Food Chem. 73, 307 (2001) http://dx.doi.org/10.1016/S0308-8146(00)00302-2[Crossref]
  • [19] H.J.D. Dorman, M. Kosar, K. Kahlos, Y. Holm, R. Hiltunen, J. Agric. Food Chem. 51, 4563 (2003) http://dx.doi.org/10.1021/jf034108k[Crossref]
  • [20] R.P. Bradley, British Herbal Compendium, (British Herbal Medicine Association, Bournemouth, 1992) Vol. 1, 99
  • [21] M. Wichtl, N.G. Bisset, Herbal Drugs and Phytopharmaceuticals (Medpharm Scientific Publishers, Stuttgart, 1994) 208
  • [22] C.A. Newall, L.A. Anderson, J.D. Phillipson, Herbal Medicines: A Guide for Health-Care Professionals (The Pharmaceutical Press, London, 1996)
  • [23] Frangulae cortex, Monographs on the Medical Uses of Plant Drugs (ESCOP, 1997)
  • [24] K. Dallenbach-Tölke, Sz. Nyiredy, G.A. Gross, O. Sticher, J. Nut. Prod. 49, 1155 (1986) http://dx.doi.org/10.1021/np50048a045[Crossref]
  • [25] R. Hänsel, L. Hörhammer, Arch. Pharm. 287, 117 (1954) http://dx.doi.org/10.1002/ardp.19542870303[Crossref]
  • [26] M. Suhaj, J. Food Compost. Anal. 19, 531 (2006) http://dx.doi.org/10.1016/j.jfca.2004.11.005[Crossref]
  • [27] A. Wojdyło, J. Oszmiański, R. Czemerys, Food Chem. 105, 940 (2007) http://dx.doi.org/10.1016/j.foodchem.2007.04.038[Crossref]
  • [28] B. Shan, Y.Z. Cai, M. Sun, H. Corke, J. Agric. Food Chem. 53, 7749 (2005) http://dx.doi.org/10.1021/jf051513y[Crossref]
  • [29] J.K.S. Moller, H.L. Madsen, T. Aaltonen, L.H. Skibsted, Food Chem. 64, 215 (1999) http://dx.doi.org/10.1016/S0308-8146(98)00143-5[Crossref]
  • [30] A. MandiĆ, S. Đilas, G. ĆetkoviĆ, J. ČanadanoviĆ-Brunet, V. Tumbas, Int. J. Food Prop. 11, 713 (2008) http://dx.doi.org/10.1080/10942910701584260[Crossref]
  • [31] R. Tsao, R. Yang, J. Chromatogr. A 1018(1) 1, 29 (2003) http://dx.doi.org/10.1016/j.chroma.2003.08.034[Crossref]
  • [32] A. Escarpa, M.C. Gonzalez, Anal. Chim. Acta 427, 119 (2001) http://dx.doi.org/10.1016/S0003-2670(00)01188-0[Crossref]
Document Type
Publication order reference
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-010-0126-8
Identifiers
JavaScript is turned off in your web browser. Turn it on to take full advantage of this site, then refresh the page.