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2010 | 8 | 4 | 861-869
Article title

Preparation and utilization of a molecularly imprinted polymer for solid phase extraction of tramadol

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Abstracts
EN
In this paper, a highly selective molecularly imprinted polymer (MIP) for tramadol hydrochloride, a drug used to treat moderate to severe pain, was prepared and its use as solid-phase extraction (SPE) sorbent was demonstrated. The molecularly imprinted solid-phase extraction procedure followed by high performance liquid chromatography with ultraviolet detector (MISPE-HPLC) was developed for selective extraction and determination of tramadol in human plasma and urine. The optimal conditions for molecularly imprinted solid-phase extraction (MISPE) consisted of conditioning with 1 mL methanol and 1 mL of deionized water at neutral pH, loading of tramadol sample (50 µg L−1) at pH 7.5, washing using 1 mL acetone and elution with 3 × 1 mL of 10% (v/v) acetic acid in methanol. The MIP selectivity was evaluated by checking several substances with similar molecular structures to that of tramadol. Results from the HPLC analyses showed that the calibration curve of tramadol (using MIP from human plasma and urine) is linear in the ranges of 6–100 and 3–120 µg L−1 with good precisions (1.9% and 2.9% for 5.0 µg L−1), respectively. The recoveries for plasma and urine samples were higher than 81%. [...]
Publisher

Journal
Year
Volume
8
Issue
4
Pages
861-869
Physical description
Dates
published
1 - 8 - 2010
online
17 - 6 - 2010
Contributors
  • Department of Chemistry, Amirkabir University of Technology, Hafez 424, Tehran, P.O. Box 15875-4413, Iran
author
  • Department of Chemistry, Amirkabir University of Technology, Hafez 424, Tehran, P.O. Box 15875-4413, Iran, majidabdouss@yahoo.com
author
  • Department of Chemistry, Amirkabir University of Technology, Hafez 424, Tehran, P.O. Box 15875-4413, Iran
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YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-010-0059-2
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