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Journal
2010 | 8 | 4 | 758-765
Article title

Controlled synthesis, characterization and thermal properties of Mg2B2O5

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EN
Abstracts
EN
Optimum conditions for synthesizing monoclinic and triclinic Mg2B2O5 compounds by high-temperature solid-state reactions were investigated. Mixtures composed of boric acid and magnesium oxide at MgO:B2O3 mole ratios of 1:0.25, 1:0.5 and 1:1.5 were heated for 1 hour at temperatures between 600–1050°C and the formed phases were identified by XRD analysis. Monoclinic Mg2B2O5 was formed by heating at 850°C for 4 hours together with minimum amounts of triclinic Mg2B2O5, while triclinic Mg2B2O5 was formed as a single phase at 1050°C for the same reaction time. The products obtained at optimum conditions were subjected to a series of tests to determine their chemical compositions, particle size distributions, surface area values, IR spectra and TG/DTA patterns. [...]
Publisher
Journal
Year
Volume
8
Issue
4
Pages
758-765
Physical description
Dates
published
1 - 8 - 2010
online
17 - 6 - 2010
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Document Type
Publication order reference
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-010-0039-6
Identifiers
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