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Journal
2010 | 8 | 3 | 662-668
Article title

Flame atomic absorption spectrometric determination of trace amounts of lead, cadmium and nickel in different matrixes after solid phase extraction on modified multiwalled carbon nanotubes

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EN
Abstracts
EN
The potential of modified multiwalled carbon nanotubes (a solid-phase extraction sorbent), for the simultaneous separation and preconcentration of lead, cadmium and nickel; has been investigated. Lead, cadmium and nickel, were adsorbed quantitatively; on modified multiwalled carbon nanotubes (in the pH range of 2–4). Parameters influencing, the simultaneous preconcentration of Pb(II), Ni(II) and Cd(II) ions (such as pH of the sample, sample and eluent flow rate, type and volume of elution solution and interfering ions), have been examined and optimized. Under the optimum experimental conditions, the detection limits of this method. for Pb(II), Ni(II) and Cd(II) ions, were 0.32, 0.17 and 0.04 ng mL−1 in original solution, respectively. Seven replicate determinations, of a mixture of 2.0 μg mL−1 lead and nickel, and 1.0 μg mL−1 cadmium; gave a mean absorbance of 0.074, 0.151 and 0.310, with relative standard deviation 1.7%, 1.5% and 1.2%, respectively. The method has been applied, to the determination of trace amounts of lead, cadmium and nickel; in biological and water samples, with satisfactory results. [...]
Publisher

Journal
Year
Volume
8
Issue
3
Pages
662-668
Physical description
Dates
published
1 - 6 - 2010
online
25 - 4 - 2010
Contributors
author
  • Department of Chemistry, Payame Noor University (PNU), Kerman, 76169-14117, Iran, szmohammadi@yahoo.com
author
  • Environment Department, Research Institute of Environmental Sciences, International Center for Science, High Technology & Environmental Sciences, Kerman, 76198-17511, Iran
author
  • Department of Chemistry, Payame Noor University (PNU), Kerman, 76169-14117, Iran
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Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-010-0029-8
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