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Journal
2010 | 8 | 1 | 155-162
Article title

Carbon ceramic electrode incorporated with zeolite ZSM-5 for determination of Piroxicam

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EN
Abstracts
EN
A new chemically modified electrode is constructed based on carbon ceramic electrode incorporated with zeolite ZSM-5. Voltammetric behavior of piroxicam at the carbon ceramic zeolite modified electrode (CCZME) was investigated. The modified electrode exhibited catalytic activity toward the electrooxidation of piroxicam. Experimental parameters such as solution pH, scan rate, concentration of piroxicam and zeolite amount were studied. It has been shown that using the CCZME, piroxicam can be determined by differential pulse voltammetry (DPV) and hydrodynamic amperometry (HA). Under the optimized conditions the calibration plots are linear in the concentration ranges of 0.20–25.00 and 0.20–50.10 μM with limit of detections of 0.65 and 0.29 μM for DPV and HA, respectively. The modified electrode with DPV and HA methods was successfully applied for analysis of piroxicam in pharmaceutical formulations. The results were favorably compared to those obtained by the spiked method. The results of the analysis suggest that the proposed method has promise for the routine determination of piroxicam in the products examined. [...]
Publisher
Journal
Year
Volume
8
Issue
1
Pages
155-162
Physical description
Dates
published
1 - 2 - 2010
online
16 - 2 - 2010
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Document Type
Publication order reference
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-009-0122-z
Identifiers
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