Comparison of solid-phase and single-drop microextractions for headspace analysis of herbal essential oils

• Authors: Martin Adam , Petr Dobiáš , Petra Pavlíková , Karel Ventura
• Languages of publication: EN

Abstracts

EN

The analytical microextraction methods of gas chromatography coupled with flame ionisation detector (GC-FID) for determination of selected essential oils in herbs were proposed. Two microextraction methods for the isolation of essential oils from plants such as Lavandula spica L., Melissa officinalis L., Mentha piperita L. and Salvia officinalis L. were used. The methods of solid-phase and single-drop microextractions, were optimised and compared. The obtained LOD values for all studied essential oils were found to be within 2.5–20.5 μg for SDME and 57.0–139.8 μg for SPME method per 100 g of dried sample leaves. The appropriate LOQ values were then 8.4–68.4 μg for SDME and 189.8–466.1 μg for SPME of target analytes per 100 g of dried sample leaves. [...]

Keywords

EN

Solid-phase microextraction; Single-drop microextraction; Gas chromatography; Essential oils; Herbs

• Publisher: De Gruyter Open
• Journal: Open Chemistry
• Year: 2009
• Volume: 7
• Issue: 3
• Pages: 303-311

Dates

published

1 - 9 - 2009

online

21 - 6 - 2009

Contributors

author

Martin Adam

• Department of Analytical Chemistry, Faculty of Chemical Technology, University of Pardubice, 532 10, Pardubice, Czech Republic

author

Petr Dobiáš

• Department of Analytical Chemistry, Faculty of Chemical Technology, University of Pardubice, 532 10, Pardubice, Czech Republic

author

Petra Pavlíková

• Department of Analytical Chemistry, Faculty of Chemical Technology, University of Pardubice, 532 10, Pardubice, Czech Republic

author

Karel Ventura

• Department of Analytical Chemistry, Faculty of Chemical Technology, University of Pardubice, 532 10, Pardubice, Czech Republic

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Identifiers

DOI

10.2478/s11532-009-0048-5