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Number of results

Journal

2009 | 7 | 3 | 362-368

Article title

Synthesis of lead-based 1212 and 3212 superconductors by an aqueous sol-gel method

Content

Title variants

Languages of publication

EN

Abstracts

EN
The aqueous sol-gel synthesis technique for the preparation of (Pb,Sr)Sr2(Y,Ca)Cu2O7±x (Pb-1212) and (Pb2,Cu)Sr2(Y,Ca)Cu2O8±x (Pb-3212) superconductors using two different complexing agents, namely 1,2-ethanediol and tartaric acid was studied. The phase transformations, composition and micro-structural features in the polycrystalline samples were studied by powder X-ray diffraction analysis (XRD), infrared spectroscopy (FTIR) and scanning electron microscopy (SEM). XRD analysis of the ceramic samples obtained by calcination of Pb-Sr-Y-Ca-Cu-O acetate-glycolate precursor gels in air, for 10 hours at 800°C and at 825°C, showed the presence of homogeneous Pb-1212 and Pb-3212 crystallites as major phases. The XRD patterns of the ceramics obtained from Pb-Sr-Y-Ca-Cu-O acetate-tartrate precursor gels, however, showed multiphasic character. The critical temperature of superconductivity (TC (onset)) observed by resistivity measurements were found to be 91 K and 75 K for Pb-1212 and Pb-3212 samples, respectively. [...]

Publisher

Journal

Year

Volume

7

Issue

3

Pages

362-368

Physical description

Dates

published
1 - 9 - 2009
online
21 - 6 - 2009

Contributors

  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania
  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania
  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania
  • Department of General and Inorganic Chemistry, Vilnius University, LT-03225, Vilnius, Lithuania

References

  • [1] G.J. Bednorz, K.A. Müller, Z. Phys. B 64, 189 (1986) http://dx.doi.org/10.1007/BF01303701[Crossref]
  • [2] D. Haught, J. Daley, P. Bakke, B. Marchionini, Int. J. Appl. Ceram. Technol. 4, 197 (2007) http://dx.doi.org/10.1111/j.1744-7402.2007.02133.x[Crossref]
  • [3] H.C. Freyhardt, Int. J. Appl. Ceram. Technol. 4, 203 (2007) http://dx.doi.org/10.1111/j.1744-7402.2007.02134.x[Crossref]
  • [4] M. Park, Y.-S. Jo, K.-S. Ryu, Int. J. Appl. Ceram. Technol. 4, 217 (2007) http://dx.doi.org/10.1111/j.1744-7402.2007.02135.x[Crossref]
  • [5] M. Murakami, Int. J. Appl. Ceram. Technol. 4, 225 (2007) http://dx.doi.org/10.1111/j.1744-7402.2007.02136.x[Crossref]
  • [6] P.N. Barnes, Int. J. Appl. Ceram. Technol. 4, 242 (2007) http://dx.doi.org/10.1111/j.1744-7402.2007.02137.x[Crossref]
  • [7] R.J. Cava et al., Nature 336, 211 (1988) http://dx.doi.org/10.1038/336211a0[Crossref]
  • [8] J.-E. Jørgensen, N.H. Andersen, Physica C 235-240, 877 (1994) http://dx.doi.org/10.1016/0921-4534(94)91663-2[Crossref]
  • [9] M.A. Subramanian et al., Physica C 157, 124 (1989) http://dx.doi.org/10.1016/0921-4534(89)90477-2[Crossref]
  • [10] J.Y. Lee, J.S. Swinnea, H. Steinfink, J. Mater. Res. 4, 763 (1989) http://dx.doi.org/10.1557/JMR.1989.0763[Crossref]
  • [11] H.K. Lee, Physica C 308, 289 (1998) http://dx.doi.org/10.1016/S0921-4534(98)00575-9[Crossref]
  • [12] T. Rouillon, M. Hervieu, B. Domenges, B. Raveau, J. Solid State Chem. 103, 63 (1993) http://dx.doi.org/10.1006/jssc.1993.1079[Crossref]
  • [13] J.S. Xue, M. Reedyk, J.E. Greedan, T. Timusk, J. Solid State Chem. 102, 492 (1993) http://dx.doi.org/10.1006/jssc.1993.1061[Crossref]
  • [14] J.-E. Jørgensen, N.H. Andersen, Physica C 218, 13 (1993)
  • [15] A. Maignan, D. Groult, R.S. Liu, T. Rouillon, P. Daniel, C. Michel, M. Hervieu, B. Raveau, J. Solid State Chem. 102, 31 (1993) http://dx.doi.org/10.1006/jssc.1993.1005[Crossref]
  • [16] M. Hechtl, J. Bernhard, K.F. Renk, Supercond. Sci. Technol. 7, 407 (1994) http://dx.doi.org/10.1088/0953-2048/7/6/013[Crossref]
  • [17] K.R. Pedersen, J.-E. Jørgensen, Physica C 264, 185 (1996) http://dx.doi.org/10.1016/0921-4534(96)00263-8[Crossref]
  • [18] J. Linden, M. Lippmaa, T. Karlemo, M. Karppinen, L. Niinistö, Supercond. Sci. Technol. 9, 399 (1996) http://dx.doi.org/10.1088/0953-2048/9/5/011[Crossref]
  • [19] M.H. Iversen, J.-E. Jørgensen, N.H. Andersen, Physica C 294, 169 (1998) http://dx.doi.org/10.1016/S0921-4534(97)01764-4[Crossref]
  • [20] H.K. Lee, J. Korean Phys. Soc. 36, 384 (2000)
  • [21] H.K. Lee, J.R. Park, Y.I. Kim, J. Korean Phys. Soc. 38, 739 (2001)
  • [22] H. Sasakura, K. Yoshida, K. Tagaya, S. Tsukui, M. Adachi, T. Oka, R. Oshima, Physica C 356, 212 (2001) http://dx.doi.org/10.1016/S0921-4534(01)00162-9[Crossref]
  • [23] J. Livage, M. Henry, C. Sanchez, Progr. Solid State Chem. 18, 259 (1988) http://dx.doi.org/10.1016/0079-6786(88)90005-2[Crossref]
  • [24] C.J. Brinker, G.W. Scherrer, Sol-Gel Science: The Physics and Chemistry of Sol-Gel Processing (Academic Press, San Diego, 1990)
  • [25] B.L. Cushing, V.L. Kolesnichenko, C.J. O’Connor, Chem. Rev. 104, 3893 (2004) http://dx.doi.org/10.1021/cr030027b[Crossref]
  • [26] A. Katelnikovas, J. Barkauskas, F. Ivanauskas, A. Beganskiene, A. Kareiva, J. Sol-Gel Sci. Techn. 41, 193 (2007) http://dx.doi.org/10.1007/s10971-006-9002-6[Crossref]
  • [27] A. Kareiva, M. Karppinen, L. Niinisto, J. Mater. Chem. 4, 1267 (1994) http://dx.doi.org/10.1039/jm9940401267[Crossref]
  • [28] A. Baranauskas, D. Jasaitis, A. Kareiva, R. Haberkorn, H.P. Beck, J. Eur. Ceram. Soc. 21, 399 (2001) http://dx.doi.org/10.1016/S0955-2219(00)00206-5[Crossref]
  • [29] S. Mathur, H. Shen, N. Lecerf, M. H. Jilavi, V. Cauniene, J.-E. Jørgensen, A. Kareiva, J. Sol-Gel Sci. Technol. 24, 57 (2002) http://dx.doi.org/10.1023/A:1015113616733[Crossref]
  • [30] A. Kareiva, I. Bryntse, M. Karppinen, L. Niinisto, J. Solid State Chem. 121, 356 (1996) http://dx.doi.org/10.1006/jssc.1996.0048[Crossref]
  • [31] A. Zalga, J. Reklaitis, E. Norkus, A. Beganskiene, A. Kareiva, Chem. Phys. 327, 220 (2006) http://dx.doi.org/10.1016/j.chemphys.2006.04.007[Crossref]
  • [32] R. Mahesh, R. Nagarajan, C.N.R. Rao, J. Solid State Chem. 96, 2 (1992) http://dx.doi.org/10.1016/S0022-4596(05)80290-7[Crossref]
  • [33] Y. Liu, Z.-F. Zhang, B. King, J. Halloran, R.M. Laine, J. Am. Ceram. Soc. 79, 385 (1996) http://dx.doi.org/10.1111/j.1151-2916.1996.tb08133.x[Crossref]
  • [34] P. Vaqueiro, M.A. Lopez-Quintela, J. Mater. Chem. 8, 161 (1998) http://dx.doi.org/10.1039/a705635d[Crossref]

Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-009-0025-z
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