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Number of results

Journal

2009 | 7 | 3 | 281-284

Article title

A hydroxyaminophosphane derived from 2-imidazolidone and its unusual structure in solution

Content

Title variants

Languages of publication

EN

Abstracts

EN
A novel hydroxyamino phosphane was synthesised through the reaction of 2-imidazolidinone with ClPPh2 and subsequently reaction of the resulting bisphosphino derivative with the Grignard reagent BrMgC5H11. The interaction of the pentyl substituent with one of the two phosphino groups and the structure in solution is shown by multinuclear NMR-spectroscopy.. [...]

Publisher

Journal

Year

Volume

7

Issue

3

Pages

281-284

Physical description

Dates

published
1 - 9 - 2009
online
21 - 6 - 2009

Contributors

author
  • Institute of Biochemistry, University of Greifswald, D-17489, Greifswald, Germany
  • Institute of Biochemistry, University of Greifswald, D-17489, Greifswald, Germany

References

  • [1] (a) O. Kühl, Coord. Chem. Rev. 250, 2867 (2006); (b) O. Kühl, Can. J. Chem. 85, 230 (2007) http://dx.doi.org/10.1016/j.ccr.2006.02.033[Crossref]
  • [2] A.M.Z. Slawin, M. Wainwright, J.D. Woollins, J. Chem. Soc., Dalton Trans. 2724 (2001) [Crossref]
  • [3] a) A.M.Z. Slawin, M. Wainwright, J.D. Woollins, New J. Chem. 24, 69 (2000); b) P. Bhattacharyya, A.M.Z. Slawin, J.D. Woollins, J. Chem. Soc., Dalton Trans. 1545 (2000); c) P. Bhattacharyya, A.M.Z. Slawin, M.B. Smith, D.J. Williams, J.D. Woollins, J. Chem. Soc., Dalton Trans. 3647 (1996) http://dx.doi.org/10.1039/a908153d[Crossref]
  • [4] a) R. Vogt, P.G. Jones, A. Kolbe, R. Schmutzler, Chem. Ber. 124, 2705 (1991); b) N. Weferling, R. Schmutzler, W.S. Sheldrick, Liebigs Ann. Chem. 167 (1982); c) G. Bettermann, R. Schmutzler, S. Pohl, U. Thewalt, Polyhedron 6, 1823 (1987); d) W.S. Sheldrick, S. Pohl, H. Zamankhan, M. Banek, D. Amiszadeh-Asl, H.W. Roesky, Chem. Ber. 114, 2131 (1981); e) C.J. Adams, M.I. Bruce, O. Kühl, B.W. Skelton, A.H. White, J. Organomet. Chem. 445, C6-C9 (1993) http://dx.doi.org/10.1002/cber.19911241211[Crossref]
  • [5] a) O. Kühl, P. Lönnecke, Inorg. Chem. 41, 4315 (2002); b) O. Kühl, W. Langel, Inorg. Chem. Comm. 6, 74 (2003); c) O. Kühl, Dalton Trans. 949 (2003); d) O. Kühl, S. Blaurock, Inorg. Chem. 43, 6543 (2004); (e) O. Kühl, S. Blaurock, T. Carls, Inorg. Chem. 45, 1723 (2006); f) O. Kühl, P. Lobitz, N. Peulecke, Phosphorus, Sulfur, and Silicon 183, 2777 (2008) http://dx.doi.org/10.1021/ic025614e
  • [6] P. Braunstein, C. Frison, X. Morise, R.D. Adams, J. Chem. Soc., Dalton Trans. 2205 (2000) [Crossref]
  • [7] a) T.Q. Ly, A.M.Z. Slawin, J.D. Woollins, Angew. Chem. 110, 2605 (1998); b) D.J. Birdsall, J. Green, T.Q. Ly, J. Novosad, M. Necas, A.M.Z. Slawin, J.D. Woollins, Z. Zak, Eur. J. Inorg. Chem. 1445 (1999) http://dx.doi.org/10.1002/(SICI)1521-3757(19980918)110:18<2605::AID-ANGE2605>3.0.CO;2-1[Crossref]
  • [8] S. Blaurock, O. Kühl, E. Hey-Hawkins, Organometallics 16, 807 (1997) http://dx.doi.org/10.1021/om9609022[Crossref]
  • [9] J.G. Verkade, L.D. Quin in: Volume 8: “Phosphorus - 31 NMR Spectroscopy in Stereochemical Analysis in A.P. Marchand (Ed.): Methods in Stereochemical Analysis (Verlag Chemie, Weinheim, 1987)
  • [10] F. Ando, H. Niwa, J. Koketsu, Chuba Daigaku Kogakubo Kiyo 24, 95 (1988)
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  • [12] J. Heinicke, R. Kadyrov, M.K. Kindermann, M. Kloss, A. Fischer, P.G. Jones, Chem. Ber. 129, 1061 (1996) http://dx.doi.org/10.1002/cber.19961290914[Crossref]
  • [13] O. Kühl, Phosphorus-31 NMR Spectroscopy - A Concise Introduction for the Synthetic Organic and Organometallic Chemist (Springer-Verlag, Heidelberg 2008)

Document Type

Publication order reference

Identifiers

YADDA identifier

bwmeta1.element.-psjd-doi-10_2478_s11532-009-0021-3
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