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Journal
2009 | 7 | 3 | 281-284
Article title

A hydroxyaminophosphane derived from 2-imidazolidone and its unusual structure in solution

Content
Title variants
Languages of publication
EN
Abstracts
EN
A novel hydroxyamino phosphane was synthesised through the reaction of 2-imidazolidinone with ClPPh2 and subsequently reaction of the resulting bisphosphino derivative with the Grignard reagent BrMgC5H11. The interaction of the pentyl substituent with one of the two phosphino groups and the structure in solution is shown by multinuclear NMR-spectroscopy.. [...]
Publisher

Journal
Year
Volume
7
Issue
3
Pages
281-284
Physical description
Dates
published
1 - 9 - 2009
online
21 - 6 - 2009
Contributors
author
  • Institute of Biochemistry, University of Greifswald, D-17489, Greifswald, Germany, dockuhl@gmail.com
  • Institute of Biochemistry, University of Greifswald, D-17489, Greifswald, Germany
References
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  • [4] a) R. Vogt, P.G. Jones, A. Kolbe, R. Schmutzler, Chem. Ber. 124, 2705 (1991); b) N. Weferling, R. Schmutzler, W.S. Sheldrick, Liebigs Ann. Chem. 167 (1982); c) G. Bettermann, R. Schmutzler, S. Pohl, U. Thewalt, Polyhedron 6, 1823 (1987); d) W.S. Sheldrick, S. Pohl, H. Zamankhan, M. Banek, D. Amiszadeh-Asl, H.W. Roesky, Chem. Ber. 114, 2131 (1981); e) C.J. Adams, M.I. Bruce, O. Kühl, B.W. Skelton, A.H. White, J. Organomet. Chem. 445, C6-C9 (1993) http://dx.doi.org/10.1002/cber.19911241211[Crossref]
  • [5] a) O. Kühl, P. Lönnecke, Inorg. Chem. 41, 4315 (2002); b) O. Kühl, W. Langel, Inorg. Chem. Comm. 6, 74 (2003); c) O. Kühl, Dalton Trans. 949 (2003); d) O. Kühl, S. Blaurock, Inorg. Chem. 43, 6543 (2004); (e) O. Kühl, S. Blaurock, T. Carls, Inorg. Chem. 45, 1723 (2006); f) O. Kühl, P. Lobitz, N. Peulecke, Phosphorus, Sulfur, and Silicon 183, 2777 (2008) http://dx.doi.org/10.1021/ic025614e
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  • [7] a) T.Q. Ly, A.M.Z. Slawin, J.D. Woollins, Angew. Chem. 110, 2605 (1998); b) D.J. Birdsall, J. Green, T.Q. Ly, J. Novosad, M. Necas, A.M.Z. Slawin, J.D. Woollins, Z. Zak, Eur. J. Inorg. Chem. 1445 (1999) http://dx.doi.org/10.1002/(SICI)1521-3757(19980918)110:18<2605::AID-ANGE2605>3.0.CO;2-1[Crossref]
  • [8] S. Blaurock, O. Kühl, E. Hey-Hawkins, Organometallics 16, 807 (1997) http://dx.doi.org/10.1021/om9609022[Crossref]
  • [9] J.G. Verkade, L.D. Quin in: Volume 8: “Phosphorus - 31 NMR Spectroscopy in Stereochemical Analysis in A.P. Marchand (Ed.): Methods in Stereochemical Analysis (Verlag Chemie, Weinheim, 1987)
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  • [13] O. Kühl, Phosphorus-31 NMR Spectroscopy - A Concise Introduction for the Synthetic Organic and Organometallic Chemist (Springer-Verlag, Heidelberg 2008)
Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-009-0021-3
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