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Journal
2009 | 7 | 3 | 322-327
Article title

Sol-gel bioactive glass-ceramics Part II: Glass-ceramics in the CaO-SiO2-P2O5-MgO system

Content
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EN
Abstracts
EN
Ceramics, with basic composition based on the CaO-SiO2-P2O5-MgO system with different Ca+ Mg/P+Si molar ratio (R), were prepared via polystep sol-gel technique. The structure of the obtained ceramic materials has been studied by XRD, FTIR spectroscopy, and SEM. X-ray diffraction showed the presence of akermanite and HA for the sample with R = 1.68 and Mg substituted β-TCP and silicocarnotite for the sample with R = 2.16, after thermal treatment at 1200°C/2 h. The obtained results are in good agreement with FTIR. In vitro test for bioactivity in static condition proved that the carbonate containing hydroxyapatite (CO3HA) can be formed on the surface of the synthesized samples. CO3HA consisted of both A- and B-type CO 32− ions. SEM micrographs depicted different forms of HA particles, precipitated on the surface after soaking in 1.5 simulated body fluid (SBF). [...]
Publisher

Journal
Year
Volume
7
Issue
3
Pages
322-327
Physical description
Dates
published
1 - 9 - 2009
online
21 - 6 - 2009
Contributors
  • University of Chemical Technology and Metallurgy, 1756, Sofia, Bulgaria, l_radev@abv.bg
  • University of Chemical Technology and Metallurgy, 1756, Sofia, Bulgaria
  • University of Chemical Technology and Metallurgy, 1756, Sofia, Bulgaria
  • University of Chemical Technology and Metallurgy, 1756, Sofia, Bulgaria
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Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-009-0014-2
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