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Journal
2009 | 7 | 1 | 143-147
Article title

Determination of penicillin V potassium in pharmaceuticals and spiked human urine by chemiluminescence

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EN
Abstracts
EN
A simple and selective method for penicillin V potassium (PVK) determination by chemiluminescence (CL) was developed. Oxidation of PVK by alkaline hydrogen peroxide produces CL, which is greatly enhanced by N, N-dimethyl formamide (DMF) and N-cetyl-N,N,N-trimethylammonium bromide (CTMAB). Optimum conditions were established using luminometry. There is a linear relationship between the chemiluminescent peak height and the amount of PVK within the range 0.5ā€“129.5 mg Lāˆ’1, with a detection limit of 0.2 mg Lāˆ’1. The coefficient of variation was 1.2% for 40 mg Lāˆ’1 PVK solution (n = 7). The method is very simple, has high sensitivity and good selectivity, and is usable for process control. It was successfully utilized for the determination of PVK in pharmaceuticals and spiked human urine. [...]
Publisher
Journal
Year
Volume
7
Issue
1
Pages
143-147
Physical description
Dates
published
1 - 3 - 2009
online
23 - 12 - 2008
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Document Type
Publication order reference
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_s11532-008-0092-6
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