2-pyrrolidone - capped Mn3O4 nanocrystals

• Authors: Tevhide Özkaya , Abdulhadi Baykal , Muhammet Toprak
• Languages of publication: EN

Abstracts

EN

Water-soluble Mn3O4 nanocrystals have been prepared through thermal decomposition in a high temperature boiling solvent, 2-pyrrolidone. The final product was characterized with XRD, SEM, TEM, FTIR and Zeta Potential measurements. Average crystallite size was calculated as ∼15 nm using XRD peak broadening. TEM analysis revealed spherical nanoparticles with an average diameter of 14±0.4 nm. FTIR analysis indicated that 2-pyrrolidone coordinates with the Mn3O4 nanocrystals only via O from the carbonyl group, thus confining their growth and protecting their surfaces from interaction with neighboring particles. [...]

Keywords

EN

Spinels; Nanocrystalline Materials; Thermal Decomposition; Mn3O4 ; Transmission Electron Microscopy (TEM)

• Publisher: De Gruyter Open
• Journal: Open Chemistry
• Year: 2008
• Volume: 6
• Issue: 3
• Pages: 465-469

Dates

published

1 - 9 - 2008

online

11 - 8 - 2008

Contributors

author

Tevhide Özkaya

• Department of Chemistry, Fatih University, 34500 Buyukcekmece, Istanbul, Turkey

author

Abdulhadi Baykal

• Department of Chemistry, Fatih University, 34500 Buyukcekmece, Istanbul, Turkey

author

Muhammet Toprak

• Department of Chemistry and Biochemistry, University of California, Santa Barbara, CA, 93106, USA

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Identifiers

DOI

10.2478/s11532-008-0041-4