Low temperature synthesis and characterization of Mn3O4 nanoparticles

• Authors: Abdülhadi Baykal , Yüksel Köseoğlu , Mehmet Şenel
• Languages of publication: EN

Abstracts

EN

Heating hydrous manganese (II) hydroxide gel at 85 °C for 12 hours produces Mn3O4 nanoparticles. They were characterized by X-ray powder diffraction (XRD) and infrared spectroscopy (FTIR). The particle size estimated from the SEM and X-ray peak broadening is approximately 32 nm, showing them to be nanocrystalline. EPR measurements confirm a typical Mn2+signal with a highly resolved hyperfine structure. [...]

Keywords

EN

Mn3O4 ; Nanoparticle; XRD; FTIR; EPR

• Publisher: De Gruyter Open
• Journal: Open Chemistry
• Year: 2007
• Volume: 5
• Issue: 1
• Pages: 169-176

Dates

published

1 - 3 - 2007

online

1 - 3 - 2007

Contributors

author

Abdülhadi Baykal

• Department of Chemistry, Fatih University, 34500, Buyukcekmec, Istanbul, Turkey

author

Yüksel Köseoğlu

• Department of Physics, Fatih University, 34500, Buyukcekmec, Istanbul, Turkey

author

Mehmet Şenel

• Department of Chemistry, Fatih University, 34500, Buyukcekmec, Istanbul, Turkey

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Identifiers

DOI

10.2478/s11532-006-0064-7