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2014 | 16 | 2 | 69-73
Article title

The Use of Ion Exchange in the Recovery of Vanadium from the Mass of a Spent Catalyst Used in the Oxidation of SO2 to SO3

Content
Title variants
Languages of publication
EN
Abstracts
EN
In the studies on the recovery of vanadium from vanadium catalyst extracts, three types of polymer strongly acidic ion exchangers were used. The ion exchange resins differed in terms of granularity and their ion exchange capacity. As a result, breakthrough curves were made for three main components of the test extract, i.e.: ions of vanadium, iron and potassium. On this basis the optimum conditions for the removal of iron ions from the solution were defined and the technological concept of the process in the semi-technical scale was proposed.
Publisher

Year
Volume
16
Issue
2
Pages
69-73
Physical description
Dates
online
26 - 6 - 2014
Contributors
  • Nicolaus Copernicus University, Faculty of Chemistry, Department of Chemical Technology, Gagarina 7, 87-100 Toruń, Poland, sebdru@uni.torun.pl
  • Nicolaus Copernicus University, Faculty of Chemistry, Department of Chemical Technology, Gagarina 7, 87-100 Toruń, Poland
  • Nicolaus Copernicus University, Faculty of Chemistry, Department of Chemical Technology, Gagarina 7, 87-100 Toruń, Poland
References
  • 1. Mazurek, K., Białowicz, K. & Trypuć, M. (2010). Recovery of vanadium, potassium and iron from a spent catalyst using urea solution. Hydrometalurgy, 103, 19–24. DOI: 10.1016/j.hydromet.2010.02.008.[Crossref]
  • 2. Grzesiak, P. (2004). Development of sulfuric acid production in Poland. Institute of Plant Protection, Poznan. [in Polish]
  • 3. Anioł, S., Korolewicz, T. & Kubala, J. (1997). Investigation concerning the recovery of V2O5 from the spent vanadium catalyst for the production of sulphuric acid, Polish Journal of Applied Chemistry, 41, 25–34.
  • 4. Mazurek, K., Białowicz, K., Trypuć, M. (2010). Extraction of vanadium compounds from the used vanadium catalyst. Polish Journal of Chemical Technology, 12(1), 23–28. DOI: 10.2478/v10026-010-0005-2.[Crossref]
  • 5. Mazurek, K. & Trypuć, M. (2009). Recovery of the components of the spent vanadium catalyst with sulphuric(VI) acid solutions. Przemysł Chemiczny, 11, 1248–1251.
  • 6. Grzesiak, P., Grobela, M., Motała, R. & Mazurek, K. (2004). Sulfuric acid – New opportunities. Institute of Plant Protection, Poznan.
  • 7. Ognyanova, A., Ozturk, A., T. De Michelis, I., Ferella, F., Taglieri, G., Akcil, A. & Veglio, F. (2009). Metal extraction from spent sulphuric acid catalyst through alkaline and acid leaching. Hydrometallurgy, 100(1–2), 20–28. DOI: 10.1016/j.hydromet.2009.09.009.[Crossref]
  • 8. Navarro, R., Guzman, J., Saucedo, I., Revilla, J., Guibal, E. (2007). Vanadium recovery from oil fly ash by leaching, precipitation and solvent extraction processes, Waste Management, 27(3), 425–438. DOI: 10.1016/j.wasman.2006.02.002.[WoS][Crossref]
  • 9. Williams, W.J. (1979). Handbook of anion determination. Butterworth and Co Ltd., London.
  • 10. Medvidović Vukojević, N., Perić, J. & Trgo, M. (2006). Column performance in lead removal from aqueous solutions by fixed bed of natural zeolite – clinoptilolite, Separation and Purification Technology, 49(3), 237–244. DOI: 10.1016/j.seppur.2005.10.005.[Crossref]
  • 11. Michaels, A.S. (1952). Simplified method of interpreting kinetic data in fluid bed ion exchange. Industry & Engineering Chemistry, 44(8), 1922–1930. DOI: 10.1021/ ie50512a049.[Crossref]
  • 12. Pawłowski, L., Klepacka, B. & Zaleski, R. (1981). A new ion exchange method for recovering highly concentrated solutions of chromates from plating effiuents, Nuclear and Chemical Waste Management, 2(1), 43–51. DOI: 10.1016/0191-815X(81)90007-3.[Crossref]
  • 13. Tomaszewska, M., Gryta, M. & Morawski, A.W. (1998). The infiuence of salt in solutions on hydrochloric acid recovery by membrane distillation, Separation and Purification Technology, 14(1–3), 183–188. DOI: 10.1016/ S1383-5866(98)00073-2.[Crossref]
  • 14. Tomaszewska, M., Gryta, M. & Morawski, A.W. (2000). Mass transfer of HCl and H2O across the hydrophobic membrane during membrane distillation, Journal of Membrane Science, 166(2), 149–157. DOI: 10.1016/ S0376-7388(99)00263-X.[Crossref]
  • 15. Tomaszewska, M. & Mientka, A. (2008). Separation of HCl from the mixture of KCl and HCl using membrane distillation, Polish Journal of Chemical Technology, 10(2), 27–32. DOI: 10.2478/v10026-008-0024-4.[Crossref]
Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.-psjd-doi-10_2478_pjct-2014-0032
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