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Journal

2005 | 3 | 4 | 830-851

Article title

A comparison of sequential extraction procedures for fractionation of arsenic, cadmium, lead, and zinc in soil

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EN

Abstracts

EN
Twelve soil samples differing in physicochemical properties and total element contents were extracted by three sequential extraction procedures to determine As, Cd, Pb, and Zn bound to individual soil fractions and are defined by individual operational procedures. In the case of arsenic, two additional sequential extraction schemes were designed entirely for fractionation of soil containing arsenic were tested. The results confirmed that determination of element proportions bound to individual soil fractions is strongly dependent on the extracting agent and/or procedure applied within individual extracting schemes. As expected, absolute values of the elements released among the individual extracting procedures are weakly comparable. More reliable results were determined for the more mobile soil elements i.e. cadmium and zinc, in the fractions characterizing the most mobile proportions of investigated elements where significant correlations with basic soil characteristics were observed. In contrast, ambiguous results were observed for As and Pb, for both the individual extraction procedures and the effect of the soil characteristics. Regardless of the studied element, the poorest results were determined for reducible and oxidizable soil fractions. The application of at least two independent procedures or modification of the extraction scheme according to element investigated and/or particular soil characteristics can also be helpful in definition of element pattern in soils in further research.

Keywords

Publisher

Journal

Year

Volume

3

Issue

4

Pages

830-851

Physical description

Dates

published
1 - 12 - 2005
online
1 - 12 - 2005

Contributors

  • Department of Agrochemistry and Plant Nutrition, Czech University of Agriculture, CZ-165 21, Prague 6- Suchdol, Czech Republic
  • Department of Agrochemistry and Plant Nutrition, Czech University of Agriculture, CZ-165 21, Prague 6- Suchdol, Czech Republic
  • Department of Agrochemistry and Plant Nutrition, Czech University of Agriculture, CZ-165 21, Prague 6- Suchdol, Czech Republic
  • Department of Agrochemistry and Plant Nutrition, Czech University of Agriculture, CZ-165 21, Prague 6- Suchdol, Czech Republic

References

  • [1] D. Chaudhuri, S. Tripathy, H. Veeresh, M.A. Powell and B.R. Hart: “Relationship of chemical fractions of heavy metals with microbial and enzyme activities in sludge and ash-amended acid lateritic soil from India”, Environ. Geol., Vol. 44, (2003), pp. 419–432. http://dx.doi.org/10.1007/s00254-003-0777-2[Crossref]
  • [2] Ş. Tokalioĝlu, Ş. Kartal and G. Birol: “Application of a three-stage sequential extraction procedure for the determination of extractable metal contents in highway soils”, Turkish J. Chem., Vol. 27, (2003), pp. 333–346.
  • [3] M. Kaasalainen and M. Yli-Halla: “Use of sequential extraction to assess metal partitioning in soils”, Environ. Poll., Vol. 126, (2003), pp. 225–233. http://dx.doi.org/10.1016/S0269-7491(03)00191-X[Crossref]
  • [4] J. Száková, P. Tlustoš, J. Balík, D. Pavlíková and V. Vaněk: “The sequential analytical procedure as a tool for evaluation of As, Cd and Zn mobility in soil”, Fresen. J. Anal. Chem., Vol. 363, (1999), pp. 594–595. http://dx.doi.org/10.1007/s002160051255[Crossref]
  • [5] J. Száková, P. Tlustoš, J. Balík, D. Pavlíková and M. Balíková: “Application of sequential extraction procedure to evaluation of influence of sewage sludge amendment on Cd and Zn mobility in soil”, Chemické Listy, Vol. 95, (2001), pp. 645–648.
  • [6] R.G. McLaren and L.M. Clucas: “Fractionation of copper, nickel, and zinc in metal-spiked sewage sludge”, J. Environ. Quality, Vol. 30 (2001), pp. 1968–1975.
  • [7] F.X. Han, A. Banin, W.L. Kingerz, G.B. Triplett, L.X. Zhou, S.J. Zheng and W.X. Ding: “New approach to studies of heavy metal redistribution in soil”, Adv. Environ. Research, Vol. 8, (2003), pp. 113–120. http://dx.doi.org/10.1016/S1093-0191(02)00142-9[Crossref]
  • [8] E. Fernández, R. Jiménez, A.M. Lallena and J. Aguilar: “Evaluation of the BCR sequential extraction procedure applied for two unpolluted Spanish soils”, Environ. Poll., Vol. 131, (2004), pp. 355–364. http://dx.doi.org/10.1016/j.envpol.2004.03.013[Crossref]
  • [9] T.T. Lim, J.H. Tay and J.Y. Wang: “Chelating-agent-enhanced heavy metal extraction from a contaminated acidic soil”, J. Environ. Engin., Vol. 130, (2004), pp. 59–66. http://dx.doi.org/10.1061/(ASCE)0733-9372(2004)130:1(59)[Crossref]
  • [10] G.M. Nystrøm, L.M. Ottosen and A. Villumsen: “The use of sequential extraction to evaluate the remediation potential of heavy metals from contaminated harbour sediment”, J. Physique IV, Vol. 107, (2003), pp. 975–978.
  • [11] A. Tessier, P.G.C. Campbell and M. Bisson: “Sequential extraction procedure for the speciation of particulate trace metals”, Anal. Chem., Vol. 51, (1979), pp. 844–851. http://dx.doi.org/10.1021/ac50043a017[Crossref]
  • [12] R.G. McLaren and D.V. Crawford: “Studies on soil copper: I. The fractionation of copper in soils”, Journal of Soil Science, Vol. 24, (1973) pp. 172–181. http://dx.doi.org/10.1111/j.1365-2389.1973.tb00753.x[Crossref]
  • [13] A.V. Filgueiras, I. Lavilla and C. Bendicho: “Chemical sequential extraction for metal partitioning in environmental solid samples”, J. Environ. Monitor., Vol. 4, (2002), pp. 823–857. http://dx.doi.org/10.1039/b207574c[Crossref]
  • [14] A.K. Chowdhury, R.G. McLaren, R.S. Swift and K.C. Cameron: “Effects of extraction period and soil-Solution ratio on the amount of zinc extracted from soils by different extractants”, Comm. Soil Sci. Plant Anal., Vol. 23, (1992) pp. 1451–1459. [Crossref]
  • [15] C.W. Gray and R.G. McLaren: “Effects of air drying or sample storage on soilsolution properties of biosolids-amended soil”, Comm. Soil Sci. Plant Anal., Vol. 34, (2003), pp. 2327–2338. http://dx.doi.org/10.1081/CSS-120024067[Crossref]
  • [16] F. Bordas and A.C.M. Bourg: “Effect of solid/liquid ratio on the remobilization of Cu, Pb, Cd and Zn from polluted river sediment”, Water Air Soil Poll., Vol. 103, (1998), pp. 137–149. http://dx.doi.org/10.1023/A:1004952608950[Crossref]
  • [17] J. Shiowatana, N. Tantidanai, S. Nookabkaew and D. Nacapricha: “A novel continuous-flow sequential extraction procedure for metal speciation in solids”, J. Environ. Quality, Vol. 30, (2001), pp. 1195–1205.
  • [18] E. Campos, E. Barahona, M. Lachica and M.D. Mingorance: “A study of the analytical parameters important for the sequential extraction procedure using microwave heating for Pb, Zn and Cu in calcareous soils”, Anal. Chim. Acta, Vol. 431, (1998), pp. 209–218.
  • [19] B. Pérez-Cid, A. Fernández-Alborés, E. Fernández-Gómez and E. Falqué-López: “Use of microwave single extractions for metal fractionation in sewage sludge samples”, Anal. Chim. Acta, Vol. 431, (2001), pp. 209–218. http://dx.doi.org/10.1016/S0003-2670(00)01335-0[Crossref]
  • [20] A.V. Filgueiras, I. Lavilla and C. Bendicho: “Comparison of the standard SM&T sequential extraction method with small-scale ultrasound-assisted single extractions for metal partitioning in sediments”, Anal. Bioanal. Chem., Vol. 374, (2002) pp. 103–108. http://dx.doi.org/10.1007/s00216-002-1427-3[Crossref]
  • [21] D. Beauchemin, K. Kyser and D. Chipley: “Inductively coupled plasma mass spectrometry with on-line leaching: A method to assess the mobility and fractionation of elements”, Anal. Chem., Vol. 74, (2002), pp. 3924–3928. http://dx.doi.org/10.1021/ac025671p[Crossref]
  • [22] W.R. MacFarlane, T.K. Kyser, D. Chipley, D. Beauchemin and C. Oates: “Continuous leach inductively coupled plasma mass spectrometry: applications for exploration and environmental geochemistry”, Geochem.-Exploration Environ. Anal., Vol. 5 (2005), pp. 123–134. http://dx.doi.org/10.1144/1467-7873/03-063[Crossref]
  • [23] P. Quevauviller, A.M. Ure, H. Muntau and B. Griepink: “Improvement of analytical measurements within the BCR-program-Single and sequential extraction procedures applied to soil and sediment analysis”, Int. J. Environ. Anal. Chem., Vol. 51, (1993), pp. 129–134. [Crossref]
  • [24] C.M. Davidson, P.C.S. Ferreira and A.M. Ure: “Some sources of variability in application of the three-stage sequential extraction procedure recommended by BCR to industrially-contaminated soil”, Fresen. J. Anal. Chem., Vol. 363, (1999), pp. 446–451. http://dx.doi.org/10.1007/s002160051220[Crossref]
  • [25] P. Quevauviller: “Operationally-defined extraction procedures for soil and sediment analysis. Part 3: New CRMs for trace-element extractable contents”, Trends Anal. Chem., Vol. 21, (2002), pp. 774–785. http://dx.doi.org/10.1016/S0165-9936(02)01105-6[Crossref]
  • [26] X.Q. Shan and C. Bin: “Evaluation of sequential extraction for speciation of tracemetals in model soil containing natural minerals and humic-acid”, Anal. Chem., Vol. 65, (1993), pp. 802–807. http://dx.doi.org/10.1021/ac00054a026[Crossref]
  • [27] A.S. Ayoub, B.A. McGaw, C.A. Shand and A.J. Midwood: “Phytoavailability of Cd and Zn in soil estimated by stable isotope exchange and chemical extraction”, Plant Soil, Vol. 252, (2003), pp. 291–300. http://dx.doi.org/10.1023/A:1024785201942[Crossref]
  • [28] K.F. Mossop and C.M. Davidson: “Comparison of original and modified BCR sequential extraction procedures for the fractionation of copper, iron, lead manganese and zinc in soils and sediments”, Anal. Chimi. Acta, Vol. 478, (2003), pp. 111–118. http://dx.doi.org/10.1016/S0003-2670(02)01485-X[Crossref]
  • [29] V.H. Kennedy, A.L. Sanchez, D.H. Oughton and A.P. Rowland: “Use of single and sequential chemical extractants to assess radionuclide and heavy metal availability from soils for root uptake”, Analyst, Vol. 122, (1997), pp. 89R-100R. http://dx.doi.org/10.1039/a704133k
  • [30] W.J.G.M. Peijnenburg and T. Jager: “Monitoring approaches to assess bioaccessibility and bioavailability of metals: Matrix issues”, Ecotox. Environ. Safe., Vol. 56, (2003), pp. 63–77. http://dx.doi.org/10.1016/S0147-6513(03)00051-4[Crossref]
  • [31] K.A. Hudson-Edwards, S.L. Houghton and A. Osborn: “Extraction and analysis of arsenic in soils and sediments”, Trends Anal. Chem., Vol. 23, (2004), pp. 745–752. http://dx.doi.org/10.1016/j.trac.2004.07.010[Crossref]
  • [32] Z. Mester, C. Cremisini, E. Ghiara and R. Morabito: “Comparison of two sequential extraction procedures for metal fractionation in sediment samples”, Anal. Chim. Acta, Vol. 359, (1998), pp. 133–142. http://dx.doi.org/10.1016/S0003-2670(97)00687-9[Crossref]
  • [33] M.B. Alvarez, M.E. Malla and D.A. Batistoni: “Comparative assessment of two sequential chemical extraction schemes for the fractionation of cadmium, chromium, lead and zinc in surface coastal sediments”, Fresen. J. Anal. Chem., Vol. 369, (2001), pp. 81–90. http://dx.doi.org/10.1007/s002160000592[Crossref]
  • [34] P. Quevauviller: “Operationally defined extraction procedures for soil and sediment analysis-I. Standardization”, Trends Anal. Chem., Vol. 17, (1998), pp. 289–298. http://dx.doi.org/10.1016/S0165-9936(97)00119-2[Crossref]
  • [35] X. Li, B.J. Coles, M.H. Ramsey and I. Thornton: “Sequential extraction of soils for multielement analysis by ICP-AES”, Chem. Geol., Vol. 124, (1995), pp. 109–123. http://dx.doi.org/10.1016/0009-2541(95)00029-L[Crossref]
  • [36] H. Zeien: Chemische Extraktionen zur Bestimmung der Bindungsformen von Schwermetallen in Böden, Thesis (PhD), 1995, Rheinische Friedrich-Wilhelms-Universität Bonn.
  • [37] W.W. Wenzel, N. Kirchbaumer, T. Prohaska, G. Stingeder, E. Lombi and D.C. Adriano: “Arsenic fractionation in soils using an improved sequential extraction procedure”, Anal. Chim. Acta, Vol. 436, (2001), pp. 1–15. http://dx.doi.org/10.1016/S0003-2670(01)00924-2[Crossref]
  • [38] J.M. Azcue, A. Mudroch, F. Rosa and G.E.M. Hall: “Effects of abandoned gold mine tailings on the arsenic concentrations in water and sediments of Jack of Clubs Lake, BC”, Environ. Tech., Vol. 15, (1994), pp. 669–678. [Crossref]
  • [39] J. Sysalová and J. Száková: “The possibilities of determination of trace element species in urban dust and aerosols”, In: Proceedings of XXXVIII seminar “Mikroelementy 2004” held at Medlov, Czech Republic, September 1 to September 3, 2004, 2theta, Český Těšín, 2004, pp. 52–56.
  • [40] J.L. Gómez-Ariza, I. Giráldez, D. Sánchez-Rodas and E. Morales: “Metal readsorption and redistribution during the analytical fractionation of tract elements in oxic estuarine sediments”, Anal. Chim. Acta, Vol. 399, (1999), pp. 295–307. http://dx.doi.org/10.1016/S0003-2670(99)00460-2[Crossref]
  • [41] C.W. Gray, R.G. McLaren, A.H.C. Roberts and L.M. Condron: “Effect of soil pH on cadmium phytoavailability in some New Zealand soils”, New Zealand Journal of Crop and Horticultural Science, Vol. 27, (1999), pp. 169–179. http://dx.doi.org/10.1080/01140671.1999.9514093[Crossref]
  • [42] C.W. Gray, R.G. McLaren, A.H.C. Roberts and L.M. Condron: “Fractionation of soil cadmium from some New Zealand soils”, Commun. Soil Sci. Plan., Vol. 31, (2000), pp. 1261–1273. [Crossref]
  • [43] L.M. Shuman: “Fractionation method for soil microelements”, Soil Sci., Vol. 140, (1985), pp. 11–22.
  • [44] M.G. Hickey and J.A. Kittrick: “Chemical partitioning of cadmium, copper, nickel and zinc in soils and sediments containing high-levels of heavy-metals”, J. Environ. Qual., Vol. 13, (1984), pp. 372–376. http://dx.doi.org/10.2134/jeq1984.133372x[Crossref]
  • [45] J.R. Bacon, I.J. Hewitt and P. Cooper: “Reproducibility of the BCR sequential extraction procedure in a long-term study of the association of heavy metals with soil components in an upland catchment in Scotland”, Sci. Total Environ., Vol. 337, (2005), pp. 191–205. http://dx.doi.org/10.1016/j.scitotenv.2004.06.010[Crossref]
  • [46] D. Leštan, H. Grěman, M. Zupan and N. Bačac: “Relationship of soil properties to fractionation of Pb and Zn in soil and their uptake into Plantago lanceolata”, Soil Sediment Contam., Vol. 12, (2003), pp. 507–522.
  • [47] C. Parat, J. Lévêque, S. Dousset, R. Chaussod and F. Andreux: “Comparison of three sequential extraction procedures used to study trace metal distribution in an acidic sandy soil”, Anal. Bioanal. Chem., Vol. 376, (2003), pp. 243–247.
  • [48] A.K. Chowdhury, R.G. McLaren, K.C. Cameron and R.S. Swift: “Fractionation of zinc in some New Zealand soils. Commun”, Commun. Soil Sci. Plan., Vol. 28, (1997), pp. 301–312. http://dx.doi.org/10.1080/00103629709369791[Crossref]
  • [49] M. Raksasataya, A.G. Langdon and N.D. Kim: “Assessment of the extent of lead redistribution during sequential extraction by two different methods”, Anal. Chim. Acta, Vol. 332, (1996), pp. 1–14. http://dx.doi.org/10.1016/0003-2670(96)00227-9[Crossref]
  • [50] E.B. Schalscha, P. Escudero and T.I. Ahumada: “Concentration and fractionation of Cu, Cr, Ni and Zn in montmorillonitic and allophanic soils: Comparison of two different extraction methods”, Agrochimica, Vol. 43, (1999), pp. 126–136.
  • [51] N.E. Keon, C.H. Swartz, D.J. Brabander, C. Harvey and H.F. Hemond: “Validation of an arsenic sequential extraction method for evaluating mobility in sediments”, Environ. Sci. Technol., Vol. 35, (2001), pp. 2778–2784. http://dx.doi.org/10.1021/es001511o[Crossref]
  • [52] M. Mihaljevič, M. Poňavič, V. Ettler and O. Šebek: “A comparison of sequential extraction techniques for determining arsenic fractionation in synthetic mineral mixtures”, Anal. Bioanal. Chem., Vol. 377, (2003), pp. 723–729. http://dx.doi.org/10.1007/s00216-003-2115-7[Crossref]
  • [53] G.E.M. Hall, J.E. Vaive, R. Beer and M. Hoashi: “Selective leaches revisited, with emphasis on the amorphous Fe oxyhydroxide phase extraction”, J. Geochem. Explor., Vol. 56, (1996), pp. 59–78. http://dx.doi.org/10.1016/0375-6742(95)00050-X[Crossref]

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bwmeta1.element.-psjd-doi-10_2478_BF02475207
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