X-ray diffraction and Mössbauer spectroscopy studies of a mechanosynthesized Fe75B25 alloy

• Authors: Elżbieta Jartych , Ludmila M. Kubalova , Victoria I. Fadeeva
• Languages of publication: EN

Abstracts

EN

In this work, the process of formation of metastable phases was investigated for the Fe75B25 composition. Mechanical synthesis was performed in a MAPF-2M high-energy planetary ball mill under an argon atmosphere. X-ray diffraction (XRD), differential scanning calorimetry (DSC), and Mössbauer spectroscopy (MS) were applied to recognize the phases. After 6 h of milling, the material consisted of two phases, that is, metastable tetragonal t-Fe2B and amorphous phases. During further thermal processing, the metastable phase was transformed into the stable Fe2B phase.

Keywords

EN

mechanosynthesis; metastable phase; Mössbauer spectroscopy; X-ray diffraction

• Publisher: De Gruyter Open
• Journal: Nukleonika
• Year: 2015
• Volume: 60
• Issue: 1
• Pages: 43-46

Dates

published

1 - 3 - 2015

online

12 - 3 - 2015

received

18 - 6 - 2014

accepted

22 - 10 - 2014

Contributors

author

Elżbieta Jartych

• Institute of Electronics and Information Technology, Lublin University of Technology, 38A Nadbystrzycka Str., 20-618 Lublin, Poland, Tel.: [phone], Fax: [phone]

author

Ludmila M. Kubalova

• Department of Chemistry, North Ossetian State University after K. L. Khetagurov, 44-46 Vatutina Str., 362025 Vladikavkaz, Russia

author

Victoria I. Fadeeva

• Department of Chemistry, M. V. Lomonosov Moscow State University, Leninsky Gory, 119899 Moscow, Russia

References

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Identifiers

DOI

10.1515/nuka-2015-0011