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Journal
2015 | 60 | 1 | 43-46
Article title

X-ray diffraction and Mössbauer spectroscopy studies of a mechanosynthesized Fe75B25 alloy

Content
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Languages of publication
EN
Abstracts
EN
In this work, the process of formation of metastable phases was investigated for the Fe75B25 composition. Mechanical synthesis was performed in a MAPF-2M high-energy planetary ball mill under an argon atmosphere. X-ray diffraction (XRD), differential scanning calorimetry (DSC), and Mössbauer spectroscopy (MS) were applied to recognize the phases. After 6 h of milling, the material consisted of two phases, that is, metastable tetragonal t-Fe2B and amorphous phases. During further thermal processing, the metastable phase was transformed into the stable Fe2B phase.
Publisher

Journal
Year
Volume
60
Issue
1
Pages
43-46
Physical description
Dates
published
1 - 3 - 2015
online
12 - 3 - 2015
received
18 - 6 - 2014
accepted
22 - 10 - 2014
Contributors
  • Institute of Electronics and Information Technology, Lublin University of Technology, 38A Nadbystrzycka Str., 20-618 Lublin, Poland, Tel.: +48 81 538 4618, Fax: +48 81 538 4312, e.jartych@pollub.pl
  • Department of Chemistry, North Ossetian State University after K. L. Khetagurov, 44-46 Vatutina Str., 362025 Vladikavkaz, Russia
  • Department of Chemistry, M. V. Lomonosov Moscow State University, Leninsky Gory, 119899 Moscow, Russia
References
  • 1. Bansal, C., Gao, Z.-Q., Hong, L. B., & Fultz, B. (1994). Phases and phase stabilities of Fe3 X alloys (X=Al, As, Ge, In, Sb, Si, Sn, Zn) prepared by mechanical alloying. J. Appl. Phys., 76, 5961–5966. DOI: 10.1063/1.358375.[Crossref]
  • 2. Kubalova, L. M., & Fadeeva, V. I. (2014). Struktura mechanosyntezirovannych splavov zheleza s p-elementami (Ai, Si, Ge, B) ekvatomnogo sostava. Izviestia RAN. Seria Fizicheskaya, 78, 131–134. DOI: 10.7868/S0367676513090251.[Crossref]
  • 3. Ackermann, M., Wagner, H.-G., Gonser, U., & Steiner, P. (1986). Bulk and surface crystallization behavior of Fe100-xBx. Hyperfine Interact., 27, 397–400. DOI: 10.1007/BF02354790.[Crossref]
  • 4. Schaaf, P., Rixecker, G., Yang, E., Wagner, C. N. J., & Gonser, U. (1994). Study on nanocrystalline and amorphous powders prepared by mechanical alloying. Hyperfine Interact., 94, 2239–2244. DOI: 10.1007/BF02063769.[Crossref]
  • 5. Del Bianco, L., Hernando, A., Bonetti, E., & Navarro, E. (1997). Grain-boundary structure and magnetic behavior in nanocrystalline ball-milled iron. Phys. Rev. B, 56, 8894–8901. DOI: 10.1103/PhysRevB.56.8894.[Crossref]
  • 6. Sanchez, F. H., Budnick, J. I., Zhang, Y. D., Hines, W. A., Choi, M., & Hasegawa, R. (1986). Mössbauer study of the local atomic environments in metastable crystalline Fe-B alloys. Phys. Rev. B, 34, 4738. DOI: 10.1103/PhysRevB.34.4738.[Crossref]
  • 7. Fernández van Raap, M. B., Sánchez, F. H., & Zhang, Y. D. (1995). On the microstructure and thermal stability of rapidly quenched Fe-B alloys in the intermediate composition range between the crystalline and amorphous states. J. Mater. Res., 10, 1919–1926. DOI: 10.1557/JMR.1995.1917.[Crossref]
Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.-psjd-doi-10_1515_nuka-2015-0011
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