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Number of results
Journal
2015 | 13 | 1 |
Article title

Titanium dioxide high aspect ratio nanoparticle hydrothermal synthesis optimization

Content
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Languages of publication
EN
Abstracts
EN
TiO2-B (bronze) nanowires were synthesized via simple hydrothermal treatment of commercial titanium dioxide nanopowder in aqueous NaOH. The reaction temperature, calcination temperature, reaction time, NaOH concentration, autoclave filing fraction and precursor were systematically varied to optimize the nanowire morphology. The crystal structure, morphology and particle size were investigated by XRD, SEM and TEM. The morphology and structure are sensitive to experimental conditions. A reaction temperature of at least 150°C and NaOH concentration at least 10 M are essential, but reaction time from 24 to 72 h makes little difference. Nanowires obtained at 150°C were 60-180 nm wide and 2-4 μm long, while those after treatment at 200°C were thinner (40-100 nm) and longer (2-6 μm). The relationship between reaction conditions and morphology is discussed and practical guidelines for titanium dioxide nanowire synthesis are suggested
EN
Keywords
Publisher

Journal
Year
Volume
13
Issue
1
Physical description
Dates
published
1 - 1 - 2015
received
17 - 9 - 2013
accepted
25 - 5 - 2014
online
9 - 10 - 2014
Contributors
  • Central Laboratory of Batteries and Cells, Institute of Non-Ferrous Metals, Division in Poznan, 61-362 Poznan, Poland
References
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Document Type
Publication order reference
Identifiers
YADDA identifier
bwmeta1.element.-psjd-doi-10_1515_chem-2015-0006
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